Preparation method of large core diameter optical fiber preform rod and optical fiber
An optical fiber preform, large core diameter technology, applied in glass manufacturing equipment, manufacturing tools, etc., can solve the problems of uneven distribution of the core refractive index, large background loss of the optical fiber, small core diameter, etc., and achieve uniform refractive index distribution, Simple preparation process
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Embodiment 1
[0059] Calculate the gaseous reaction material Al(acac) according to the formula composition requirements of the large core diameter optical fiber preform core 3 , POCl 3 、SiCl 4 、Yb(thd) 3 and SiF 4 and set the flow rate of the gaseous reaction material in the MCVD automatic control software, as shown in Table 1; connect the quartz tube to the MCVD deposition lathe, preheat the quartz tube with a hydrogen-oxygen flame, and pass it into SF after the preheating is completed. 6 The gas erodes the inner wall of the quartz tube. After the erosion, the gas material is passed into the quartz tube according to the set flow value to start depositing the core layer; during the deposition process, the heating temperature of the quartz tube is 1850 ° C, and the rotation speed of the tube is 30 rpm. The moving speed of the oxyhydrogen flame is 100mm / min; after the deposition is finished, the Cl 2 Shrunk quartz tube, Cl 2 The flow rate is 5mL / min. After the hollow tube has been shrunk...
Embodiment 2
[0064] According to the component flow rate of the optical fiber preform in embodiment one and the refractive index profile of the preform, adjust the component Al(acac) 3 , POCl 3 、Yb(thd) 3 or SiF 4 The flow rate is set in the MCVD automatic control software. The set values are shown in Table 2; SF 6 The gas erodes the inner wall of the quartz tube; after the erosion, the gas material is passed into the quartz tube according to the set flow value to start depositing the core layer; during the deposition process, the heating temperature of the quartz tube is 1850 ° C, and the rotation speed of the tube is 30 rpm minutes, the moving speed during the oxyhydrogen flame deposition process is 100mm / min; 2 Shrunk quartz tube, Cl 2 The flow rate is 5mL / min. After the hollow tube has been shrunk several times and fired into a solid rod, the optical fiber preform is flame-polished at 1600°C. The prepared large-core optical fiber preform was fused at high temperature, and its r...
Embodiment 3
[0069] According to the formula component requirements of the large-diameter optical fiber preform core, combined with the component flow rate and refractive index distribution results of the optical fiber preform in Example 1, each of the deposition layers set in the MCVD automatic control software in this embodiment The flow values of the components are shown in Table 3; after the setting is completed, the quartz tube is connected to the MCVD deposition lathe, and the quartz tube is preheated by the hydrogen-oxygen flame. After the preheating is completed, the SF 6 The gas erodes the inner wall of the quartz tube; after the erosion, the gas material is passed into the quartz tube according to the set flow value to start depositing the core layer; during the deposition process, the heating temperature of the quartz tube is 1900 ° C, and the rotation speed of the tube is 30 rpm Minutes, the moving speed of the oxyhydrogen flame is 100mm / min; after the deposition is completed,...
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