Antibacterial emulsion for fresh keeping of var. ramosa Hort. and method for preparing var. ramosa Hort. fresh keeping film
A fresh-keeping film and lettuce technology, which is applied in the preservation of fruits and vegetables, protection of fruits/vegetables with a protective layer, and application, can solve the problems of poor dispersion of emulsion, unstable coating, short fresh-keeping period, etc., and achieve stable film formation. , The effect of enhancing the stability of the coating and the strong antibacterial ability
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Embodiment 1
[0026] 1. Preparation of carbon quantum dots: Dissolve 0.2-0.5g of urea phosphate, 0.3-0.6g of citric acid and 875-1000μL of ethylenediamine in 25-50mL of deionized water. Then the above solution was transferred to a microwave digestion tank, sealed and placed in a microwave digestion apparatus. The temperature program was set as follows: the reaction temperature was raised to 150° C. within 1 min, and the temperature was kept constant for 30 min. After cooling to room temperature, the obtained clear and transparent solution was centrifuged at 10000rpm for 15-20min. Finally, the supernatant was dried in a vacuum oven at 60° C. to obtain the final product.
[0027] 2. Preparation of propolis extract: crush and sieve the frozen propolis, then mix it with 75% ethanol solution at a material-to-liquid ratio of 1:15-20, extract at 40-45°C for 24 hours, and keep stirring. Then ultrasonically treat the leached propolis solution at 40-45°C for 15-20 minutes, then perform suction filt...
Embodiment 2
[0035] 1. Preparation of carbon quantum dots: same as in Example 1
[0036] 2, preparation of propolis extract: with embodiment 1
[0037] 3. The preparation method of plant essential oil antibacterial coating packaging film:
[0038] (1) Mix 0.5g sweet orange essential oil and 3mL glycerin, heat up to 40-60°C, mix and stir for 20-40min, and record it as the oil phase;
[0039] (2) Mix 0.05g of carbon quantum dots and 95mL of distilled water, stir and dissolve at room temperature, and record it as the water phase;
[0040] (3) Add the water phase prepared in step (2) to the oil phase prepared in step (1), add 1g Tween 80 at the same time, stir at 40-50°C for 30-50min, fully dissolve the mixture, emulsify and homogenize, Get plant essential oil antibacterial lotion;
[0041] (4) The fresh-keeping antibacterial emulsion of lettuce prepared in step (3) is prepared with sterile water to prepare a dilution of concentration 0.5%, and the prepared propolis extract is prepared into...
Embodiment 3
[0044] 1. Preparation of carbon quantum dots: same as in Example 1
[0045] 2, preparation of propolis extract: with embodiment 1
[0046] 3. The preparation method of plant essential oil antibacterial coating packaging film:
[0047] (1) Mix 0.7g cinnamon oil and 4mL propylene glycol, heat up to 40-60°C, mix and stir for 20-40min, and record it as the oil phase;
[0048] (2) Mix 0.05g of carbon quantum dots and 90mL of distilled water, stir and dissolve at room temperature, and record it as the water phase;
[0049] (3) Add the water phase prepared in step (2) to the oil phase prepared in step (1), add 0.7g of Span 80 at the same time, stir at 40-50°C for 30-50min, fully dissolve the mixture, emulsify and homogenize , to obtain plant essential oil antibacterial emulsion;
[0050] (4) The fresh-keeping antibacterial emulsion of lettuce prepared in step (3) is prepared with sterile water to prepare a dilution of concentration 0.6%, and the prepared propolis extract is prepar...
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