Technological preparation method of anti-virus oral liquid
An antiviral oral liquid and preparation technology, applied in the field of traditional Chinese medicine, can solve the problems of complete loss of volatile components, unsatisfactory inclusion effect, low water solubility of volatile oil, etc., to achieve guaranteed curative effect, high encapsulation efficiency, and equipment The effect of less investment
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Embodiment 1
[0032] The preparation method of antiviral oral liquid, concrete process step is as follows:
[0033] (1) Pretreatment of traditional Chinese medicine raw materials: Weigh 900g isatis root, 400g gypsum, 200g patchouli, 225g rehmannia glutinosa, 175g turmeric, 425g reed rhizome, 175g Shichangpu, 175g Anemarrhena anemarrhena, 325g forsythia Below 10mm, mix well and set aside;
[0034] (2) Distillation and extraction: Use steam distillation to distill and extract the above-mentioned mixed medicinal materials after crushing, add 8 times the amount of pure water to the mixed medicinal materials and mix them, and keep a slight boil under the condition of steam pressure 0.05-0.10Mpa after boiling State for 1.5 hours, collect 1964mL of volatile oil emulsion;
[0035] Then add 6 times the amount of purified water to the obtained dregs, boil it and keep it in a slightly boiling state for 1 hour and 20 minutes under the condition of steam pressure of 0.01-0.05Mpa, and filter and combine...
Embodiment 2
[0043] Embodiment 2: preparation method is basically the same as embodiment 1, difference is:
[0044] Step (5) volatile oil clathrate treatment:
[0045]Take 10 g of water-soluble cyclodextrin and add an appropriate amount of distilled water to prepare a saturated solution, then add the volatile oil emulsion collected in step (2), place it in an ultrasonic instrument, and place it at a temperature of 45-52°C for 30-60 minutes;
[0046] After adding a small amount of absolute ethanol solution, place it at a temperature of 45°C, add an appropriate amount of colloidal silica in small amounts for several times, stir and grind while adding, and grind until it becomes a paste, continue grinding for 20-30 minutes, and filter with suction , the resulting clathrate was rinsed with absolute ethanol, dried at 40°C to obtain a powdery volatile oil clathrate, and the mass of the clathrate was weighed.
Embodiment 3
[0047] Embodiment 3: The preparation method is basically the same as in Example 1, the difference is that the volatile oil emulsion obtained in step (2) is directly subjected to inclusion treatment: first, the volatile oil content in the volatile oil emulsion is measured and measured;
[0048] Take 50g of water-soluble cyclodextrin and add an appropriate amount of distilled water to prepare a saturated solution, then add the volatile oil emulsion collected in step (2), place it in an ultrasonic instrument, and place it at 50°C for 30 minutes;
[0049] After adding 40mL of absolute ethanol solution, place it at 45°C, add 15g of colloidal silicon dioxide in small amounts for several times, stir and grind while adding, and grind until it becomes a paste, continue grinding for 30min, and filter with suction. The compound was rinsed with absolute ethanol and dried at 40°C to obtain a powdery volatile oil clathrate, and the mass of the clathrate was weighed.
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