Functional fiber and microfluidic spinning device and fiber preparing method thereof

A spinning device and microfluidic control technology, applied in stretch spinning, fiber treatment, fiber chemical characteristics, etc., can solve the problems of high requirements for equipment and production environment, long time consumption in the transfer process, and difficulty in realizing fiber design, etc. , to achieve the effect of easy promotion, easy integration and easy operation

Active Publication Date: 2019-03-26
QINGDAO UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The phase separation method is to obtain a nanoporous foam through several steps such as dissolution, gelation, extraction, coagulation and drying, and the solid polymer is transferred into the foam pores to obtain polymer nanofibers; like the self-assembly method, its The disadvantage is that the transfer process takes too long
Mechanical stretching can produce very long single fiber filaments, but only those viscoelastic materials that can withstand large enough stress stretching deformation may use this method, which limits the range of applications
The operation method of electrospinning method is relatively simple, and it can continuously spin fiber filaments, but it has high requirements for equipment and production environment, and poor controllability. fiber for design

Method used

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  • Functional fiber and microfluidic spinning device and fiber preparing method thereof
  • Functional fiber and microfluidic spinning device and fiber preparing method thereof
  • Functional fiber and microfluidic spinning device and fiber preparing method thereof

Examples

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preparation example Construction

[0040] A microfluidic spinning preparation method of a structure controllable function designable fiber of the present invention comprises the following steps:

[0041] (1) The spinning solution or coagulation solution with a mass fraction of 0.1-30% is poured into the spinning tank sequentially, and left to stand for degassing for 0.5-3 hours to obtain the spinning solution or coagulation solution for microfluidic spinning;

[0042] (2) The computer 1 controls the propeller of the spinning pot through the solenoid valve 2, and the speed of the propeller is 0.05-100mm / min, so as to realize the design of the fiber components online;

[0043] (3) The spinning solution or coagulation solution enters the microfluidic spinning chip through the spinning solution pipeline at a flow rate of 0.1-100mL / min, and converges in the common spinning solution pipeline 14 to form nascent fibers;

[0044] (4) The as-spun fibers are drawn through the airflow gathering drafting zone 13, and after ...

Embodiment 1

[0051] See attached figure 1 , a microfluidic spinning preparation method of a structure controllable function designable fiber of the present invention, comprising the following steps:

[0052] 1) According to the structure of the designed functional fiber, the microfluidic chip 12 is taken, and the microfluidic chip 12 has six spinning solution pipelines, which are respectively the first spinning solution pipeline 5, the second spinning solution pipeline 6, and the third spinning solution pipeline. The spinning solution pipeline 7, the fourth spinning solution pipeline 8, the fifth spinning solution pipeline 9, and the sixth spinning solution pipeline 10, these six spinning solution pipelines are all connected with the common spinning solution pipeline 14;

[0053] The six spinning liquid pipelines of the microfluidic chip 12 are all provided with corresponding spinning pots and propellers connected with the spinning pots, which are respectively the first propeller and the s...

Embodiment 2

[0065] On the basis of Example 1, the components of the spinning solution, the mass concentration, the speed of the propeller, the flow rate of the spinning solution and the flow through the pipeline were adjusted.

[0066] In this embodiment, the spinning solution includes spinning solution A and spinning solution B, and the spinning solution A is a chitosan solution with a mass concentration of 2%, and its preparation method is: take chitosan, dissolve in 5% In the acetic acid aqueous solution, stand defoaming to obtain chitosan solution; the spinning solution B is a graphene solution with a mass fraction of 0.1%, and its preparation method is: take a certain amount of self-made graphene and dissolve it in water, and ultrasonically disperse it for 10 minutes to obtain graphene solution.

[0067] In the present embodiment, in the present embodiment, the spinning solution A is packed into the second propeller and the spinning tank in the spinning tank 16 and the third propelle...

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Abstract

The invention discloses a functional fiber and a microfluidic spinning device and fiber preparing method thereof. The microfluidic spinning device comprises a control mechanism, a nascent fiber forming mechanism, an airflow gathering drafting mechanism and an after-finishing and winding mechanism. The fiber preparing method includes the steps that spinning liquid or solidification liquid is sequentially injected into a spinning can, and standing defoaming is carried out; fiber constituent designing is online achieved through a control mechanism; the spinning liquid or the solidification liquidenters a microfluidic spinning chip through spinning liquid pipes, is converged in a public spinning liquid pipe, and is collected to form a nascent fiber; the nascent fiber is drafted through the airflow gathering drafting mechanism, solidified and dried through a fiber heating drier in sequence, and is wound to a winding roller finally, and the structure-controllable and function-devisable fiber is obtained. According to the microfluidic spinning device, the structure of the fiber is designed through programming, a preparing method is controllable, a complex structure and the multifunctionality which are difficult to achieve with other spinning methods are achieved, the preparing process is simple, repeatability is good, and application fields are broad.

Description

technical field [0001] The present invention relates to the technical field of microfluidic spinning, in particular to a microfluidic spinning device for fibers with controllable structure and designable functions, a method for preparing fibers spun on the device and the obtained structure controllable functions Designable fibers. Background technique [0002] The structure of the fiber determines some properties of the fiber to a certain extent. For example, the cross section of the cotton fiber is round and hollow inside. This structure makes the cotton fiber have good warmth retention, air permeability, hygroscopicity and dyeing performance; the cross section of the silk is Composed of two silk fibroin coated with sericin, the special structure formed by the triangular cross-section of silk fibroin and the lamellar structure of sericin makes silk have a luster that cannot be compared with other fibers. In order to obtain the good properties of this kind of natural fibers...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D01D1/09D01D5/14D01D5/253D01D5/30D01D5/34D01D5/32D01F8/18D01F8/16D01F8/12
CPCD01D1/09D01D5/14D01D5/253D01D5/30D01D5/32D01D5/34D01F8/12D01F8/16D01F8/18
Inventor 田明伟胡希丽曲丽君朱士凤张宪胜刘士广孙亚宁
Owner QINGDAO UNIV
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