Metal doped ferrite nano material and preparation method of magnetic nano particles containing same and application thereof
A technology of magnetic nanoparticles and metal doping, applied in biochemical equipment and methods, preparations for in vivo experiments, magnetic materials, etc., can solve the problems of low longitudinal relaxation rate, transverse longitudinal relaxation rate ratio, etc.
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0115] (1) Weigh 1g of NaOH in a 100ml beaker, add 10ml of oleic acid and 10ml of ethanol therein, and stir on a magnetic stirrer until the NaOH is dissolved and dispersed evenly to obtain solution a;
[0116] (2) Weigh 1.73mM Fe 2+ Salt and 0.267mM Zn 2+ Salt, dissolved in 20ml ultrapure water, and ultrasonicated until all the salt is dissolved and mixed evenly to obtain solution b;
[0117] (3) At room temperature, the above solution b was added dropwise to solution a, and magnetically stirred until the solution turned brown and clear, to obtain solution c;
[0118](4) Take 30ml of c solution and transfer it to a polytetrafluoroethylene liner, put it in a reactor and seal it, put the reactor into an oven, and react at a constant temperature of 230°C for 15 hours;
[0119] (5) After the reaction is completed, the reactor is cooled to room temperature, and the nanoparticles at the bottom of the polytetrafluoroethylene liner are dissolved in chloroform and taken out into a 50...
Embodiment 2
[0126] (1) Weigh 1g of NaOH in a 100ml beaker, add 10ml of oleic acid and 10ml of ethanol therein, and stir on a magnetic stirrer until the NaOH is dissolved and dispersed evenly to obtain solution a;
[0127] (2) Weigh 1.73mM Fe 2+ Salt and 0.534mM Zn 2+ Salt, dissolved in 20ml ultrapure water, and ultrasonicated until all the salt is dissolved and mixed evenly to obtain solution b;
[0128] (3) At room temperature, the above solution b was added dropwise to solution a, and magnetically stirred until the solution turned brown and clear, to obtain solution c;
[0129] (4) Take 30ml of c solution and transfer it to a polytetrafluoroethylene liner, put it in a reactor and seal it, put the reactor into an oven, and react at a constant temperature of 230°C for 15 hours;
[0130] (5) After the reaction is completed, the reactor is cooled to room temperature, and the nanoparticles at the bottom of the polytetrafluoroethylene liner are dissolved in chloroform and taken out into a 5...
Embodiment 3
[0138] (1) Weigh 1g of NaOH in a 100ml beaker, add 10ml of oleic acid and 10ml of ethanol therein, and stir on a magnetic stirrer until the NaOH is dissolved and dispersed evenly to obtain solution a;
[0139] (2) Weigh 1.73mM Fe 2+ Salt and 0.801mM Zn 2+ Salt, dissolved in 20ml ultrapure water, and ultrasonicated until all the salt is dissolved and mixed evenly to obtain solution b;
[0140] (3) At room temperature, the above solution b was added dropwise to solution a, and magnetically stirred until the solution turned brown and clear, to obtain solution c;
[0141] (4) Take 30ml of c solution and transfer it to a polytetrafluoroethylene liner, put it in a reactor and seal it, put the reactor into an oven, and react at a constant temperature of 230°C for 15 hours;
[0142] (5) After the reaction is completed, the reactor is cooled to room temperature, and the nanoparticles at the bottom of the polytetrafluoroethylene liner are dissolved in chloroform and taken out into a 5...
PUM
Login to view more Abstract
Description
Claims
Application Information
Login to view more - R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap