Coating composition for chemical drug-resistant polyolefin material and preparation method thereof
A technology of chemical resistance and polyolefin, applied in the direction of coating, etc., can solve the problems of unsatisfactory chemical resistance of coating film, achieve good chemical resistance, ensure appearance color and chemical resistance, improve reaction interaction The effect of link density
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example 1
[0032] Add glycidyl methacrylate, vinyl chloride monomer, vinyl acetate monomer, hydroxyethyl methacrylate or hydroxyethyl acrylate, azobisisobutyronitrile, solvent methyl ethyl ketone and methyl isobutyronitrile to the four-necked flask in turn. Butyl ketone, and use nitrogen replacement to remove the air in the reaction flask, and use nitrogen protection, heat up to 60-90 ° C, condense and reflux for 4-8 hours to obtain the above-mentioned glycidyl methacrylate modified vinyl chloride / acetic acid Ethylene Copolymer Resin 1. Wherein, the molar ratio of glycidyl methacrylate, vinyl chloride monomer, vinyl acetate monomer and hydroxyethyl acrylate is 0.1-0.4:0.4-0.8:1:0.1-0.2. The amount of azobisisobutyronitrile is 0.1-0.5% of the total mass of the above monomers. The liquid acid value of the vinyl chloride / vinyl acetate copolymer resin 1 modified by glycidyl methacrylate is 2.4 KOHmg / g, and the weight average molecular weight of the copolymer resin 1 detected by GPC is 75,00...
example 2
[0034] Add glycidyl methacrylate, vinyl chloride monomer, vinyl acetate monomer, hydroxyethyl acrylate, azobisisobutyronitrile, solvent ethyl ketone, and methyl isobutyl ketone to a four-necked flask in sequence, and use nitrogen gas to The air in the reaction bottle was replaced and removed, protected with nitrogen, heated to 60-90° C., condensed and refluxed for 4-8 hours to obtain the above-mentioned glycidyl methacrylate modified vinyl chloride / vinyl acetate copolymer resin 2. Wherein, the molar ratio of glycidyl methacrylate, vinyl chloride monomer, vinyl acetate monomer and hydroxyethyl acrylate is 0.4-0.8:0.1-0.4:1:0.1-0.2. The amount of azobisisobutyronitrile is 0.1-0.5% of the total mass of the above monomers. The liquid acid value of the copolymer resin 2 of vinyl chloride / vinyl acetate modified by glycidyl methacrylate is 5.0 KOHmg / g, and the weight average molecular weight of the copolymer resin 1 detected by GPC is 82000.
example 3
[0036] Add glycidyl methacrylate, vinyl chloride monomer, vinyl acetate monomer, hydroxyethyl methacrylate, azobisisobutyronitrile, solvent ethyl ketone and methyl isobutyl ketone successively in the four-necked flask, and Use nitrogen replacement to remove the air in the reaction bottle, and use nitrogen protection, heat up to 60-90 ° C, condense and reflux for 4-8 hours to obtain the above-mentioned glycidyl methacrylate modified vinyl chloride / vinyl acetate copolymer resin 3. Wherein, the molar ratio of glycidyl methacrylate, vinyl chloride monomer, vinyl acetate monomer, and hydroxyethyl methacrylate is 0.01-0.04:0.4-0.8:1:0.1-0.2. The amount of azobisisobutyronitrile is 0.1-0.5% of the total mass of the above monomers. The liquid acid value of the vinyl chloride / vinyl acetate copolymer resin 3 modified by glycidyl methacrylate is 0.3 KOHmg / g, and the weight average molecular weight of the copolymer resin 1 detected by GPC is 78,000.
[0037] The brief molecular framewor...
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