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High-strength and high-toughness silicon carbide ceramic bearing plate, manufacturing method and application thereof

A high-toughness silicon carbide and silicon carbide ceramic technology, applied in the direction of working carrier, can solve the problems of high-precision silicon wafer, low thermal conductivity of corundum disk, low service life of carrier disk, etc., and achieve good chemical corrosion resistance. , The effect of thickness reduction and process manufacturing cost reduction

Pending Publication Date: 2019-05-28
NANTONG SANZER PRECISION CERAMICS CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, at present, the specific rigidity of the corundum carrier plate is low, the thickness is large, and its strength and toughness are low, so it is easy to be damaged by bumps during use.
At the same time, due to the certain corrosive effect of the polishing liquid, the service life of the carrier plate is relatively low, and the accuracy usually decreases within half a year, requiring rework
Especially as the diameter of the silicon wafer increases, the corundum disk is prone to thermal deformation due to its low thermal conductivity, which has a greater impact on high-precision silicon wafers

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0048] A high-strength and high-toughness silicon carbide ceramic carrier disc, the production material of the silicon carbide ceramic carrier disc includes the following components by mass:

[0049] 70 parts of silicon carbide; 10 parts of silicon carbide whiskers;

[0050] 1 part of tungsten carbide; 5 parts of boron carbide;

[0051] 1 part of binder; 10 parts of lubricant.

[0052] Further, in step a, the particle size of silicon carbide powder is 0.2 μm; the particle size of silicon carbide whiskers is 5.0 μm, and the aspect ratio is 20; the particle size of tungsten carbide powder is 3.0 μm, and the particle size of boron carbide powder is The particle size is 0.1 μm.

[0053] Further, in step b, the binder is phenolic resin, and the lubricant is liquid paraffin.

[0054] A method for manufacturing a high-strength and high-toughness silicon carbide ceramic carrier disc, the steps of the method are:

[0055]a. Ingredients and mixing: add 70 parts by mass of silicon ca...

Embodiment 2

[0066] A high-strength and high-toughness silicon carbide ceramic carrier disc, the production material of the silicon carbide ceramic carrier disc includes the following components by mass:

[0067] 95 parts of silicon carbide; 2 parts of silicon carbide whiskers;

[0068] 15 parts of tungsten carbide; 0.5 parts of boron carbide;

[0069] 10 parts of binder; 0.5 parts of lubricant.

[0070] The difference between this embodiment and Embodiment 1 is that in step a, the particle size of silicon carbide powder is 0.8 μm; the particle size of silicon carbide whiskers is 0.1 μm, and the aspect ratio is 70; the particle size of tungsten carbide powder is The particle size of the boron carbide powder is 0.1 μm, and the particle size of the boron carbide powder is 1.5 μm; in step e, the maximum sintering temperature is 2300° C., and the holding time is 0.5 hours. The density of the silicon carbide ceramic carrier plate obtained in this embodiment is 96.6%, the bending strength is 4...

Embodiment 3

[0072] A high-strength and high-toughness silicon carbide ceramic carrier disc, the production material of the silicon carbide ceramic carrier disc includes the following components by mass:

[0073] 75 parts of silicon carbide; 8 parts of silicon carbide whiskers;

[0074] 3 parts of tungsten carbide; 4 parts of boron carbide;

[0075] 2 parts of binder; 9 parts of lubricant.

[0076] The difference between this embodiment and Embodiment 1 is that in step a, the particle size of the silicon carbide powder is 0.3 μm; the particle size of the silicon carbide whiskers is 4 μm, and the aspect ratio is 60; the particle size of the tungsten carbide powder is is 2 μm, and the particle size of the boron carbide powder is 1 μm; in step e, the maximum sintering temperature is 2140° C., and the holding time is 1 hour. The density of the silicon carbide ceramic carrier plate obtained in this embodiment is 94.7%, the bending strength is 460MPa, and the fracture toughness is K IC 4.1MPa...

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Abstract

The invention discloses a high-strength and high-toughness silicon carbide ceramic bearing plate, a manufacturing method and application thereof. The silicon carbide ceramic bearing plate is preparedfrom the following materials in parts by mass: 70-95 parts of silicon carbide, 2-10 parts of silicon carbide whiskers, 1 to 15 parts of tungsten carbide, 0.5 to 5 parts of boron carbide, 1 to 10 partsof a binder and 0.5 to 10 parts of a lubricant. The manufacturing method comprises burdening, mixing, pulping, spray drying, isostatic pressing, sintering and finish machining. The silicon carbide ceramic bearing plate is applied to the assembly of chemical-mechanical polishing devices. According to the silicon carbide ceramic bearing plate made by the manufacturing method, the strength and toughness are greatly superior to a common corundum ceramic bearing plate at present; a ceramic bearing plate with the same size can be reduced by 1 / 3 in thickness; the ceramic bearing plate is applied tothe chemical-mechanical polishing devices, the stability in the polishing process is greatly improved, the reliability in the operation process is greatly increased, the service life of the ceramic bearing plate is greatly prolonged, and the process manufacturing cost is reduced.

Description

technical field [0001] The invention relates to a carrier plate, a manufacturing method and an application, in particular to a high-strength and high-toughness silicon carbide ceramic carrier plate, a manufacturing method and an application. Background technique [0002] Chemical Mechanical Polishing (CMP) is an important process for obtaining high-precision silicon wafers in semiconductor manufacturing. It mainly uses the chemical reaction between the silicon wafer material and the oxidant and catalyst in the polishing liquid to form a soft layer that is relatively easy to remove, and then removes the soft layer under the mechanical action of the abrasive in the polishing liquid and the polishing pad. The surface of the workpiece is exposed again, and then the chemical reaction is carried out, so that the surface polishing of the silicon wafer is completed in the alternating process of chemical action and mechanical action. [0003] In the CMP process, the silicon wafer is...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B35/577C04B35/81C04B35/622C04B35/634B24B37/27
Inventor 闫永杰
Owner NANTONG SANZER PRECISION CERAMICS CO LTD
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