Preparation method of natural nano-functional finishing agent for silk

A nano-functional and finishing agent technology, applied in fiber treatment, biochemical fiber treatment, improved hand-feeling fibers, etc., can solve problems such as single function, environmental pollutants, physical health damage, etc., to improve functional characteristics and improve softness. , the effect of improving the stability

Inactive Publication Date: 2019-07-02
SUZHOU INST OF TRADE & COMMERCE
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Traditional fabrics have relatively simple functions after finishing, and most of the commonly used finishing...

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] The preparation method of silk natural nano functional finishing agent comprises the following steps:

[0025] (1) Preparation of finishing agent A liquid: under the condition of nitrogen protection, add 15 parts of dried polyethylene glycol into a four-neck round bottom flask, and then add deionized water 4 times the weight of polyethylene glycol, Then add 12 parts of diphenylmethane diisocyanate and 2-3 drops of dibutyltin dilaurate catalyst, slowly raise the temperature to 90 ° C under stirring conditions, and then add 22 parts of TiO 2 , 18 parts of ZnO and 15 parts of SiO 2 The mixed nanoparticles formed, keep the temperature and continue stirring for 2.5 hours, then lower the reaction temperature to room temperature, add 30 parts of ethanol, then slowly add 8 parts of sodium bisulfite aqueous solution, and then ultrasonically disperse it for 15 minutes to obtain the finished product. Agent A liquid;

[0026] (2) Preparation of finishing agent B liquid: finishing...

Embodiment 2

[0037] The preparation method of silk natural nano functional finishing agent comprises the following steps:

[0038] (1) Preparation of finishing agent A liquid: under the condition of nitrogen protection, add 10 parts of dried polyethylene glycol into a four-neck round bottom flask, and then add deionized water 3 times the weight of polyethylene glycol, Then add 8 parts of diphenylmethane diisocyanate and 2-3 drops of dibutyltin dilaurate catalyst, slowly raise the temperature to 80 ° C under stirring conditions, and then add 15 parts of TiO 2 , 10 parts of ZnO and 10 parts of SiO 2 The mixed nano-particles formed, keep the temperature and continue to stir the reaction for 2 hours, then lower the reaction temperature to room temperature, add 20 parts of ethanol, then slowly add 5 parts of sodium bisulfite aqueous solution, and then ultrasonically disperse it for 10 minutes to obtain the finishing agent A liquid;

[0039] (2) Preparation of finishing agent B liquid: finishi...

Embodiment 3

[0050] The preparation method of silk natural nano functional finishing agent comprises the following steps:

[0051] (1) Preparation of finishing agent A liquid: under the condition of nitrogen protection, add 12 parts of dried polyethylene glycol into a four-neck round bottom flask, and then add 3.5 times the weight of polyethylene glycol in deionized water, Then add 10 parts of diphenylmethane diisocyanate and 2-3 drops of dibutyltin dilaurate catalyst, slowly raise the temperature to 85 ° C under stirring conditions, and then add 20 parts of TiO 2 , 15 parts of ZnO and 12 parts of SiO 2 The mixed nanoparticles formed were kept at this temperature and continued to stir for 2.3 hours, then the reaction temperature was lowered to room temperature, 25 parts of ethanol was added, and then 6 parts of sodium bisulfite aqueous solution was slowly added, and it was ultrasonically dispersed for 12 minutes to obtain the finished product. Agent A liquid;

[0052] (2) Preparation of ...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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PUM

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Abstract

The invention provides a preparation method of a natural nano-functional finishing agent for silk. The natural nano-functional finishing agent for the silk is prepared from finishing agent liquid A, finishing agent liquid B, finishing agent liquid C and finishing agent liquid D, wherein the finishing agent liquid A is prepared from modified nano-particles, the finishing agent liquid B is preparedfrom a silane coupling agent, the finishing agent liquid C is mixed liquid of natural extracts and modified silicon emulsion, and the finishing agent liquid D is prepared from glutaraldehyde. During fabric finishing, the liquid B firstly reacts with the fabric, the liquid A is then used for treating, and the liquid D is cross-linked on the fabric by using the liquid C. Compared with the untreatedfabric, the fabric treated by using the finishing agent has higher ultraviolet resistance, softness, wrinkle resistance, antistatic property, yellowing resistance and antibacterial property; therefore, the finishing agent has an important application value in the aspect of silk fabric finishing.

Description

technical field [0001] The invention belongs to the technical field of textiles, and in particular relates to a preparation method of a silk natural nanometer functional finishing agent. Background technique [0002] Silk is soft to the touch, has good moisture absorption and air permeability, and is comfortable to wear. It is a kind of fabric that is favored by people. However, silk has the defects of easy wrinkling and shrinkage, which affects the wearing performance of silk. Therefore, people have been focusing on the research on the wrinkle resistance of silk for a long time. [0003] However, with the improvement of people's living standards, people's requirements for clothing are getting higher and higher, and multifunctional fabrics have become the trend of future development. The functions of traditional fabrics after finishing are relatively single, and most of the commonly used finishing agents are environmental pollutants, which have brought great harm to human l...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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IPC IPC(8): D06M15/647D06M11/46D06M11/44D06M11/79D06M13/513D06M13/00D06M15/00D06M13/123D06M101/10
CPCD06M11/44D06M11/46D06M11/79D06M13/00D06M13/123D06M13/513D06M15/00D06M15/647D06M16/00D06M2101/10D06M2200/20D06M2200/25D06M2200/50
Inventor 虞琳凌瑶时倩陆涛许磊
Owner SUZHOU INST OF TRADE & COMMERCE
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