A kind of method for preparing lithium manganese phosphate/graphene nanosheets in aqueous system
A graphene nanosheet, lithium manganese phosphate technology, applied in graphene, phosphate, nanocarbon and other directions, can solve the problems of difficult to achieve industrialization, high temperature and pressure, harsh reaction conditions, etc., to shorten the transmission distance, reduce Effect of surface tension, mild reaction conditions
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0025] Step S1: Dissolve 0.15 mol of lithium hydroxide in 30 mL of deionized water to obtain solution A, add 0.05 mol of manganese acetate and 0.05 mol of phosphoric acid into 70 mL of deionized water, then add 19.6 mg of graphene oxide and ultrasonically disperse to obtain a solution containing graphene oxide solution B, add 1mL of alkyl glucoside nonionic surfactant APG06 and solution A to solution B in sequence under stirring;
[0026] Step S2: Place the reaction solution obtained in step S1 in a reaction vessel with a reflux device, and place it under N 2 Under protection, reflux reaction at 100°C for 25h, and the obtained precipitate was centrifuged at 8000r / min, washed with deionized water and vacuum-dried at 80°C for 12h to obtain lithium manganese phosphate / graphene nanosheets. In the lithium manganese phosphate / graphene nanosheets The content of graphene is 1wt%.
[0027] XRD analysis proves that the lithium manganese phosphate in the target product is pure olivine p...
Embodiment 2
[0029] Step S1: Dissolve 0.15 mol of lithium hydroxide in 30 mL of deionized water to obtain solution A, add 0.05 mol of manganese acetate and 0.05 mol of phosphoric acid into 70 mL of deionized water, then add 9.8 mg of graphene oxide and ultrasonically disperse to obtain a solution containing graphene oxide solution B, add 3mL of alkyl glucoside non-ionic surfactant APG0810 and solution A to solution B in sequence under stirring;
[0030] Step S2: Place the reaction solution obtained in step S1 in a reaction vessel with a reflux device, and place it under N 2 Reflux reaction at 100°C for 36h under protection, and the resulting precipitate was centrifuged at 8000r / min, washed with deionized water and vacuum-dried at 80°C for 12h to obtain lithium manganese phosphate / graphene nanosheets. In the lithium manganese phosphate / graphene nanosheets The content of graphene is 0.5wt%.
[0031] XRD analysis proves that the lithium manganese phosphate in the target product is pure olivi...
Embodiment 3
[0033] Step S1: Dissolve 0.3 mol of lithium hydroxide in 30 mL of deionized water to obtain solution A, add 0.1 mol of manganese chloride and 0.1 mol of phosphoric acid into 70 mL of deionized water, then add 19.6 mg of graphene oxide and ultrasonically disperse to obtain a solution containing graphite oxide Solution B of alkenes, add 2mL of alkyl glucoside nonionic surfactant APG1214 and solution A to solution B in sequence under stirring;
[0034] Step S2: Place the reaction solution obtained in step S1 in a reaction vessel with a reflux device, and place it under N 2 Reflux reaction at 100°C for 48h under protection, and the resulting precipitate was centrifuged at 8000r / min, washed with deionized water and vacuum-dried at 100°C for 12h to obtain lithium manganese phosphate / graphene nanosheets. In the lithium manganese phosphate / graphene nanosheets The content of graphene is 0.5wt%.
[0035] XRD analysis proves that the lithium manganese phosphate in the target product is ...
PUM
| Property | Measurement | Unit |
|---|---|---|
| thickness | aaaaa | aaaaa |
| thickness | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More