Aqueous formaldehyde-free painting pigment and preparation method thereof
A formaldehyde and painting technology, applied in the field of water-based formaldehyde-free painting pigments and their preparation, can solve the problems of high pigment manufacturing cost, dermatitis, aquatic toxicity, etc. Effect
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[0031] A preparation method of water-based formaldehyde-free paint, comprising the following steps:
[0032] S1, mixing the toner, vegetable gum and surfactant and then grinding to make a color paste;
[0033] S2, adding inorganic electrolyte and inorganic thickener to the color paste, stirring, and then sterilizing at 120-130°C, and dispersing and activating under the conditions of vacuum pressure 0.7-0.9KPa and rotating speed 400-500r / min after the sterilization is completed; and
[0034] S3, after the dispersion and activation is completed, lower the temperature to below 40°C, add the antibacterial agent, and stir evenly to obtain the finished product.
[0035] Grinding in the present invention is to use a three-roll mill to achieve a specified fineness through the mutual extrusion of the surfaces of three horizontal rollers and friction at different speeds to make a color paste, and the fineness in the present invention is less than 10 μm.
[0036] The method of the prese...
Embodiment 1
[0041] 10 mass parts of toner, 60 mass parts of vegetable gum (gum arabic, peach gum and pectin are the mixture of 1:1.2:1.5 in mass ratio) and 3.5 mass parts of surfactant (hexadecyl trimethyl ammonium chloride) mixed and ground to make a color paste with a fineness of 10 microns;
[0042] Add 0.05 parts by mass of inorganic electrolyte sodium chloride and 1 part by mass of inorganic thickener (bentonite, attapulgite and aluminum silicate at a mass ratio of 1:1.2:2) to the color paste, stir evenly, and then Sterilize at 120°C. After the sterilization is completed, disperse and activate for 25 minutes under the conditions of vacuum pressure 0.7KPa and rotation speed 400r / min;
[0043] After dispersing and activating, lower the temperature to 40°C, add 0.05 parts by mass of antibacterial agent chlorphenesin, and stir evenly to obtain a finished product.
Embodiment 2
[0045] 15 parts by mass of toner, 65 parts by mass of vegetable gum (gum arabic and carrageenan in a mass ratio of 1:1) and 5.5 parts by mass of surfactant (octadecylamine acetate) mixed Grinding to make a color paste with a fineness of 5 microns;
[0046] Add 0.15 parts by mass of inorganic electrolyte potassium chloride and 1 part by mass of inorganic thickener (bentonite, attapulgite and aluminum silicate at a mass ratio of 1:1.5:3) to the color paste, stir evenly, and then Sterilize at 130°C. After the sterilization is completed, disperse and activate for 30 minutes under the conditions of vacuum pressure 0.9KPa and rotation speed 500r / min;
[0047] After dispersing and activating, lower the temperature to 30°C, add 0.1 parts by mass of antibacterial agent paraben, and stir evenly to obtain a finished product.
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