Method for recovering uranium oxide from uranium containing wastewater
A uranium oxide and wastewater technology, applied in chemical instruments and methods, uranium oxides/hydroxides, alkali metal oxides/hydroxides, etc., can solve the problems of low efficiency, difficult industrialization, restrictions, etc., and achieve convenient recovery , The effect of simple process flow and convenient detection
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[0029] Example 1
[0030] First prepare polystyrene aldehyde-based microspheres:
[0031] (1) Mix 18 mL of isopropanol and 2.5 g of polyvinylpyrrolidone PVP dispersant, ultrasonically assisted dissolving, add it to a three-necked flask equipped with a condenser, and place it in a 70℃ constant temperature water bath, mechanically stir and maintain the speed 315 r / min;
[0032] (2) Dissolve 0.1 g of azobisisobutyronitrile AIBN initiator in 6 mL of styrene to prepare a styrene solution with the initiator dissolved;
[0033] (3) Add the styrene solution with initiator dissolved in (2) to the system obtained in (1), stir and mix well for 30 minutes, then add 3 mL of acrolein C 3 H 4 O, react at a constant temperature at 70°C for 8 h. After the reaction is stopped, the polystyrene aldehyde-based sphere emulsion is prepared by ultrasonic centrifugation and washing three times with ethanol and water, and polystyrene aldehyde-based microspheres are obtained after drying.
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