High-hardness edge-sealing silane-modified polyether sealant and preparation method thereof
A technology of silane-modified polyether and edge silane, which is applied in the direction of polyether adhesives, chemical instruments and methods, adhesives, etc., can solve the problem of low hardness of rubber strips, achieve fast curing speed, increase hardness density, and hard surface smooth effect
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[0022] Example 1
[0023] In the embodiment of the present invention, a high-hardness edge-sealing silane-modified polyether sealant has a sealing hardness of 88-90 Shore A after being cured. The sealant includes the following raw materials in parts by weight: silane-modified polyether pre- Polymer: 15 parts, plasticizer: 13 parts; Reinforcing and increasing powder: 57.5-66.5 parts; Antioxidant: 0.5 part; Cross-linking agent: 1.5 part; Coupling agent: 0.6 part; Catalyst: 0.05 part; High styrene resin: 4 parts.
[0024] The silane-modified polyether prepolymer is a siloxane-terminated modified polyether resin.
[0025] The plasticizer is one or more of diisodecyl phthalate (DIDP), diisononyl phthalate (DINP) and polyether polyol (PPG).
[0026] The reinforcing and increasing powder is one or several mixed powders of nanometer calcium carbonate, heavy calcium carbonate or titanium dioxide.
[0027] The described antioxidant is β-(3,5-di-tert-butyl-4-hydroxyphenyl) octadecyl p...
Example Embodiment
[0034] Example 2
[0035] In the embodiment of the present invention, a high-hardness edge-sealing silane-modified polyether sealant has a sealing hardness of 88 Shore A, and the sealant includes the following raw materials in parts by weight: silane-modified polyether resin: 15 parts, o-phenylene Diisononyl diformate (DINP): 13 parts, nano calcium carbonate: 18 parts, heavy calcium carbonate: 48 parts, titanium dioxide: 1.5 parts, β-(3,5-di-tert-butyl-4-hydroxybenzene base) octadecyl propionate: 0.5 part, vinyltrimethoxysilane: 1.5 part, N-(β-aminoethyl)-γ-aminopropyltrimethoxysilane 0.6 part, dilaurate dilaurate Butyl tin: 0.05 part, 4 parts of HS-85 high styrene resin.
[0036] Prepare as follows:
[0037] 1) Weigh the weight of each raw material according to the required proportion;
[0038] 2), the weighed diisononyl phthalate DINP plasticizer, nano calcium carbonate, heavy calcium carbonate, titanium dioxide reinforcing powder, high styrene resin and β-(3,5 -Di-tert-...
Example Embodiment
[0040] Example 3
[0041] A high-hardness edge-sealing silane-modified polyether sealant. After curing, the sealing hardness reaches 90 Shore A. The sealant includes the following raw materials in parts by weight: silane-modified polyether resin: 15 parts, phthalic acid Diisononyl ester (DINP): 13 parts, nano calcium carbonate: 25 parts, heavy calcium carbonate: 40 parts, titanium dioxide: 1.5 parts, β-(3,5-di-tert-butyl-4-hydroxyphenyl) Octadecyl propionate: 0.5 part, vinyltrimethoxysilane: 1.5 part, N-(β-aminoethyl)-γ-aminopropyltrimethoxysilane 0.6 part, dibutyltin dilaurate: 0.05 part, 4 parts of HS-85 high styrene resin.
[0042] Prepare as follows:
[0043] 1) Weigh the weight of each raw material according to the required proportion;
[0044]2) First, mix the well-weighed reinforced and incremental powders of nano-calcium carbonate, heavy calcium carbonate, and titanium dioxide, and then put them into an oven, and keep the temperature at 110-120 °C for 12 hours, so t...
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