Moisture-preserving flower nutrient soil and preparing method thereof
A flower nutrient soil, nitrogen protection technology, applied in the directions of botanical equipment and methods, culture medium, planting substrate, etc., can solve the problems of poor scour resistance, water retention and drought resistance of flower nutrient soil, and achieve increased moisturizing performance and enhanced water absorption. performance effect
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preparation example Construction
[0031] The preparation method of carrying surfactant is:
[0032](1) Take 11-bromo-1-undecanol and mix it with isopropanol according to the mass ratio of 1~3:8~10, then add dropwise chlorosulfonic acid with 45~55% of the mass of 11-bromo-1-undecanol, Control the dropping time for 30-50 minutes, stir and mix at 25-30°C for 20-30 minutes to obtain a mixed solution, take the mixed solution and add 20% sodium carbonate aqueous solution with a mass fraction of 4-8:2-5, and adjust the pH to 8~9, stir and mix for 30~50min, and rotovap to get rotovap, set aside;
[0033] (2) Take selenium powder and add deionized water according to the mass ratio of 5~10:100~150, stir and mix at 25~30°C for 10~20min, then add sodium borohydride with 90~95% of the quality of selenium powder, and pass in nitrogen protection , stir and mix at 25-30°C for 20-30min to obtain a stirred mixture, take the stirred mixture and add selenium powder at a mass ratio of 100-150:3-9, heat up to 60-70°C and stir and ...
Embodiment 1
[0046] The preparation method of carrying surfactant is:
[0047] (1) Take 11-bromo-1-undecanol and add isopropanol to mix according to the mass ratio of 1:8, then add dropwise chlorosulfonic acid with 45% mass of 11-bromo-1-undecanol, and control the dropping time for 30 minutes. Stir and mix at 25°C for 20 minutes to obtain a mixed solution. Take the mixed solution and add 20% sodium carbonate aqueous solution with a mass fraction of 4:2, adjust the pH to 8, stir and mix for 30 minutes, and rotavap to obtain a rotovap, which is set aside;
[0048] (2) Take selenium powder and add deionized water at a mass ratio of 5:100, stir and mix at 25°C for 10 minutes, then add sodium borohydride with 90% of the mass of the selenium powder, pass in nitrogen protection, stir and mix at 25°C for 20 minutes, and stir For the mixture, take the stirred mixture and add selenium powder in a mass ratio of 100:3, heat up to 60°C and stir and mix for 20 minutes to obtain a mixture;
[0049] (3) ...
Embodiment 2
[0061] The preparation method of carrying surfactant is:
[0062] (1) Take 11-bromo-1-undecanol and mix it with isopropanol according to the mass ratio of 2:9, then add dropwise chlorosulfonic acid with 50% mass of 11-bromo-1-undecanol, and control the dropping time for 40 minutes. Stir and mix at 28°C for 25 minutes to obtain a mixed solution. Take the mixed solution and add 20% sodium carbonate aqueous solution with a mass fraction of 7:4, adjust the pH to 8.5, stir and mix for 40 minutes, and rotate to evaporate to obtain a rotary evaporator, which is set aside;
[0063] (2) Take selenium powder and add deionized water according to the mass ratio of 8:130, stir and mix at 28°C for 15 minutes, then add sodium borohydride with a mass of 93% of the selenium powder, pass through nitrogen protection, stir and mix at 28°C for 25 minutes, and stir For the mixture, take the stirred mixture and add selenium powder in a mass ratio of 130:7, heat up to 65°C and stir and mix for 30 min...
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