Quartz glass and ultraviolet emitting element member using same
A technology of quartz glass and straight lines, applied in the field of components for ultraviolet light-emitting elements, can solve problems such as low productivity, achieve the effects of suppressing deterioration and good laser processability
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[0112] (example 1)
[0113] The above-mentioned steps 1 to 8 are carried out to obtain quartz glass.
[0114] In step 1, the purity is 99.9% or more, the average particle size is 20nm, and the specific surface area is 90m using an ultrasonic homogenizer. 2 33.9 parts by mass of the raw material silica powder per g was dispersed in 66.1 parts by mass of water whose pH was adjusted to 13 using a pH adjuster as a solvent to prepare a dispersion.
[0115] In step 2, 88.2 parts by mass of the above-mentioned dispersion liquid, 10.0 parts by mass of the water-soluble epoxy resin, and 1.8 parts by mass of the aliphatic amine curing agent are mixed and defoamed by a vacuum pump-equipped rotating and revolving mixer to prepare a mixed liquid.
[0116] In step 3, the above-mentioned mixed liquid is filled in a polyethylene mold of 30 mm×10 mmt in diameter.
[0117] In step 4, the mixed solution filled in the mold is allowed to stand at room temperature to be solidified.
[0118] After taking out t...
Example
[0139] (Example 2)
[0140] In step 7, the molded body degreased in step 6 was fired in the atmosphere at 1125°C instead of vacuum firing. Except for step 7, the same steps as in Example 1 were implemented.
Example
[0141] (Example 3)
[0142] In step 1, the purity is 99.9% or more, the average particle size is 100nm, and the specific surface area is 55~65m using an ultrasonic homogenizer. 2 62.9 parts by mass of raw material silica powder per g and 37.1 parts by mass of water whose pH was adjusted to 13 with a pH adjuster as a solvent were dispersed to prepare a dispersion.
[0143] In step 2, 94.1 parts by mass of the above-mentioned dispersion, 5.0 parts by mass of the water-soluble epoxy resin, and 0.9 parts by mass of the aliphatic amine curing agent are mixed and defoamed using a rotating and revolving mixer equipped with a vacuum pump to prepare a mixed solution.
[0144] In the following steps, the same steps as in Example 1 were implemented to obtain quartz glass.
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