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Wormwood micropowder composite acrylic fiber polymer material fiber and preparation method thereof

A technology of polymer materials and micropowder, which is applied in the fields of fiber chemical characteristics, rayon manufacturing, and conjugated synthetic polymer rayon, etc. It can solve the problems of difficult control of grafting rate and low proportion of effective products.

Inactive Publication Date: 2019-09-17
ZHONGKE TEXTILE RES INST QINGDAO CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

The surface of this method is completely composed of protein molecules, which has good human affinity, hygroscopicity and antistatic properties, but its grafting rate is difficult to control, and the proportion of effective products obtained is low

Method used

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  • Wormwood micropowder composite acrylic fiber polymer material fiber and preparation method thereof
  • Wormwood micropowder composite acrylic fiber polymer material fiber and preparation method thereof
  • Wormwood micropowder composite acrylic fiber polymer material fiber and preparation method thereof

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Embodiment 1

[0037] Embodiment 1 A kind of wormwood micropowder composite acrylic polymer material fiber and its preparation method

[0038] The present invention provides a method for preparing acrylic polymer fiber composited with wormwood micropowder, the method comprising: preparation of modified polyacrylonitrile spinning solution, preparation, blending and spinning of wormwood micropowder; specifically:

[0039] (1) Preparation of modified polyacrylonitrile spinning solution

[0040] Mix commercially available polyacrylonitrile P30T powder, ethanol and water-soluble polylactic acid multi-block polycarbonate, dissolve in solvent dimethylformamide to form modified polyacrylonitrile spinning solution;

[0041] The polyacrylonitrile P30T powder has a relative density of 1.12, a molecular weight Mw of 95000, and a moisture content of 0.01%;

[0042] The water-soluble polylactic acid multi-block polycarbonate has a weight average molecular weight of 59300-61000 (gel permeation chromatogra...

Embodiment 2

[0059] Embodiment 2 A kind of wormwood micropowder composite acrylic polymer material fiber and its preparation method

[0060] The present invention also provides a preparation method of wormwood micropowder composite acrylic polymer fiber, said method comprising: preparation of modified polyacrylonitrile spinning solution, preparation, blending and spinning of wormwood micropowder; specifically:

[0061] (1) Preparation of modified polyacrylonitrile spinning solution

[0062] Mix commercially available polyacrylonitrile P30T powder, ethanol and water-soluble polylactic acid multi-block polycarbonate, dissolve in solvent dimethylformamide to form modified polyacrylonitrile spinning solution;

[0063] The polyacrylonitrile P30T powder has a relative density of 1.12, a molecular weight Mw of 10000-11000, and a moisture content of ≤1%;

[0064] The water-soluble polylactic acid multi-block polycarbonate has a weight average molecular weight of 79800-81200 (gel permeation chroma...

Embodiment 3

[0081] Embodiment 3 A kind of wormwood micropowder composite acrylic polymer material fiber and its preparation method

[0082] The present invention also provides a preparation method of wormwood micropowder composite acrylic polymer fiber, said method comprising: preparation of modified polyacrylonitrile spinning solution, preparation, blending and spinning of wormwood micropowder; specifically:

[0083] (1) Preparation of modified polyacrylonitrile spinning solution

[0084] Mix commercially available polyacrylonitrile P30T powder, ethanol and water-soluble polylactic acid multi-block polycarbonate, dissolve in solvent dimethylformamide to form modified polyacrylonitrile spinning solution;

[0085] The polyacrylonitrile P30T powder has a relative density of 1.12, a molecular weight Mw of 98500-10000, and a moisture content of ≤1%;

[0086] The water-soluble polylactic acid multi-block polycarbonate has a weight average molecular weight of 66800-70700 (gel permeation chroma...

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Abstract

The invention provides a preparation method of a wormwood micropowder composite acrylic fiber polymer material fiber. The method comprises the steps of preparation of a modified polyacrylonitrile spinning solution and preparation, blending and spinning forming of wormwood micropowder. According to the wormwood micropowder composite acrylic fiber polymer material fiber, the breaking strength is 7.66-8.24 cN / dtex, the elongation at break is 56.8-59.2%, the breaking strength after 800-hour solarization is 7.12-7.95 cN / dtex, the rebound rate when the fiber is elongated by 20% is 82.5-94.0%, and the dry wear-resisting number is 1998-2011. The fiber has different degrees of inhibition effect on aspergillus niger, gold alpha-hemolytic streptococcus, diplococcus pneumoniae, corynebacterium diphtheriae, sonne bacillus, typhoid and paratyphoid bacillus, vibrio cholerae and the like; the moisture regain rate of a fabric prepared from the fiber is 1.98-2.01%, and the anti-pilling level of the fabric is higher than level 4.

Description

technical field [0001] The invention belongs to the technical field of textile materials and relates to a composite polymer material fiber, in particular to a wormwood micropowder composite acrylic fiber polymer material fiber and a preparation method thereof. Background technique [0002] Acrylic fiber, that is, polyacrylonitrile fiber, is known as artificial wool. It has the advantages of softness, easy dyeing and light resistance. The softening temperature of fiber is 190-230℃, it can resist acid, oxidant and general organic solvent, but its alkali resistance is poor. [0003] The invention of patent No. CN200810064708.8 provides a method for processing acrylic fibers, which dips acrylic fibers in a chemical bath for 10-15s at room temperature, then puts them into boiling water and washes them for 10-15s, then dries them, and then rinses them in 100-120 Drying at ℃ for 15-20min completes the modification of the acrylic fiber surface; wherein the chemical bath consists o...

Claims

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Application Information

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IPC IPC(8): D01F8/08D01F8/16D01F1/10
CPCD01F1/10D01F1/103D01F8/08D01F8/16
Inventor 黄效华黄效谦刘宇刘洁黄效龙甄丽
Owner ZHONGKE TEXTILE RES INST QINGDAO CO LTD
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