Multi-layer building roof heat-preservation waterproof coiled material and preparation method thereof
A waterproof membrane, multi-layer technology, applied in the direction of construction, building structure, roofing, etc., can solve the problems that anti-aging agents cannot meet the anti-aging, affect the performance of PVC materials, and poor anti-aging performance, so as to prevent ultraviolet aging, Achieve heat retention effect and inhibit oxidation effect
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Embodiment 1
[0022] The specific preparation process of the antioxidant is as follows: ① Weigh 15g of mercaptosuccinic acid and add it to 300mL of ether and stir to dissolve it, then add 26.2g of thionyl chloride to it, raise the temperature to 70-80°C and stir for 5-6h, then depressurize Distill to obtain mercaptosuccinyl chloride; ②Add 9.4g phenol and 150mL ethanol to the reaction vessel at the same time, then add 0.94g potassium carbonate to it, stir and mix for 3-5min, then add 11.5g mercaptosuccinyl chloride to it, stir and react at room temperature for 8 -10h, then the obtained product was evaporated to remove the solvent therein to obtain a powder product, the powder was added to water and stirred for 2-3min, then filtered and dried to obtain product A; ③ 10g of obtained product A and 200mL nitrobenzene were simultaneously Put it into the reaction vessel, add 4.5g aluminum chloride and 2.1g titanium tetrachloride to the reaction vessel at the same time, raise the temperature to 165°C...
Embodiment 2
[0024]The specific preparation process of the polyvinyl chloride waterproof layer is as follows: 800g of polyvinyl chloride and 10g of the antioxidant prepared in Example 1 were simultaneously added to the internal mixer for 60-70min mastication, and the obtained material was mixed with 20g of quartz powder, 10g of hard Fatty acid, 70g of polydimethylsiloxane, 30g of carbon black and 20g of plasticizer were extruded into a screw extruder to obtain a polyvinyl chloride waterproof layer with a thickness of 0.9mm.
Embodiment 3
[0026] The specific preparation process of the polyvinyl chloride waterproof layer is the same as in Example 2, and the antioxidant prepared in Example 1 used in Example 2 is replaced by the anti-aging agent IPPSI.
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Abstract
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