A method for preparing magnetic adsorption material from animal and plant waste
A technology for magnetic adsorption materials, animals and plants, applied in chemical instruments and methods, adsorption water/sewage treatment, alkali metal compounds, etc. The effects of biodegradability, high internal structure retention, and strength regeneration
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Embodiment 1
[0026] Step 1. The bagasse is sheared and pulped (the ratio of bagasse to water is 1:10), and 100 parts by weight of the crude fiber slurry obtained by filtering is added to 100 parts by weight of 64% sulfuric acid aqueous solution, and processed by mechanical stirring for 2 hours. Cellulose nanocrystals were obtained by centrifugal washing and separation.
[0027] Step 2. 20 parts by weight of cellulose nanocrystals are dispersed in 100 parts by weight, 4 parts by weight of surfactants and 2 parts by weight of pore-forming agents and 5 parts by weight of calcium acetate, mechanically stirred for 2 hours, and added 5 parts by weight of concentration of 10% sodium phosphate aqueous solution, mechanical stirring, centrifugal washing, separation and drying to obtain a hydroxyapatite fiber composite material, and continuous heat treatment for 3 hours in an oxygen atmosphere of 180 ° C, and collecting powder to obtain hollow hydroxyapatite.
[0028] Step 3. Disperse 40 parts by wei...
Embodiment 2
[0031] Step 1. The bagasse is sheared and pulped (the ratio of bagasse to water is 1:10), and 200 parts by weight of the crude fiber slurry obtained by filtering is added to 100 parts by weight of 64% sulfuric acid aqueous solution, and processed by mechanical stirring for 4 hours. Cellulose nanocrystals were obtained by centrifugal washing and separation.
[0032] Step 2. 40 parts by weight of cellulose nanocrystals are dispersed in 100 parts by weight, 6 parts by weight of surfactants and 4 parts by weight of pore-forming agents and 10 parts by weight of calcium acetate, mechanically stirred for 6 hours, and added 10 parts by weight of concentration of 10% sodium phosphate aqueous solution, mechanical stirring, centrifugal washing, separation and drying to obtain a hydroxyapatite fiber composite material, in an oxygen atmosphere of 200 ° C, continuous heat treatment for 5 hours, collecting powder to obtain hollow hydroxyapatite.
[0033] Step 3. Disperse 60 parts by weight o...
Embodiment 3
[0036] Step 1. The bagasse is sheared and pulped (the ratio of bagasse to water is 1:10), and 100 parts by weight of the crude fiber slurry obtained by filtering is added to 100 parts by weight of 64% sulfuric acid aqueous solution, and processed by mechanical stirring for 4 hours. Cellulose nanocrystals were obtained by centrifugal washing and separation.
[0037]Step 2. 20 parts by weight of cellulose nanocrystals are dispersed in 100 parts by weight, 6 parts by weight of surfactants and 2 parts by weight of pore-forming agents and 5 parts by weight of calcium acetate, mechanically stirred for 2 hours, and add 10 parts by weight of concentration of 10% sodium phosphate aqueous solution, mechanical stirring, centrifugal washing, separation and drying to obtain a hydroxyapatite fiber composite material, in an oxygen atmosphere of 190 ° C, continuous heat treatment for 4 hours, collecting powder to obtain hollow hydroxyapatite.
[0038] Step 3. Disperse 40 parts by weight of ho...
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