Environment-friendly gunpowder for fireworks and firecrackers
A technology for firecrackers and fireworks, which is applied in the direction of nitrating acyclic/alicyclic/heterocyclic amine explosive compositions, etc., can solve problems such as slight smoke and environmental impact, and achieve the effect of reducing fire hazards
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Embodiment 1
[0022] Example 1: The molecular formula of silver nitrotetrazole is CHN 5 AgO 2 ,
[0023] Its structural formula is shown in the figure:
[0024] Preparation method: Dissolve 10 grams of 5-aminotetrazole in 150 milliliters of water and heat to 75 degrees Celsius. Dissolve 22 grams of sodium nitrite in 150 milliliters of water and heat to 60 degrees Celsius. Slowly drop 1 g of sodium nitrite solution into the 5-aminotetrazole solution, raise the temperature of the mixed solution to 80°C and keep it for 1 hour. While stirring, 107 milliliters of 1.1 molar silver nitrate solution was added to the mixed solution to produce a yellow-white precipitate, which was naturally cooled to room temperature and filtered by suction to obtain silver nitrotetrazole.
Embodiment 2
[0025] Embodiment two: the molecular formula of copper nitrotetrazole is CHN 5 CuO 2 ,
[0026] Its structural formula is shown in the figure:
[0027] Preparation method: Dissolve 10 grams of 5-aminotetrazole in 150 milliliters of water and heat to 75 degrees Celsius. Dissolve 22 grams of sodium nitrite in 150 milliliters of water and heat to 60 degrees Celsius. The sodium nitrite solution was slowly dropped into the 5-aminotetrazole solution, and the temperature of the mixed solution was raised to 80°C and kept for 1 hour to obtain a sodium nitrotetrazole solution. Add 12 grams of cuprous chloride to 100 ml of water, add sodium nitrotetrazole solution while stirring, heat up to reflux temperature, react for 2 hours, naturally cool to room temperature, filter with suction, and dry in an oven at 50 degrees to obtain nitro Copper tetrazolium.
[0028] Among them, the compound containing both azo functional group and tetrazole functional group in the tetrazole compound is...
Embodiment 3
[0029] Example 3: The molecular formula of 5,5'-azotetrazole zinc salt is C 2 N 10 Zn,
[0030] Its structural formula is shown in the figure:
[0031] Preparation method: Dissolve 10 grams of 5,5'-azotetrazole sodium salt and 11 grams of barium chloride in 100 ml of water to form a 5,5'-azotetrazole barium precipitate, vacuum filter, and remove the precipitate The substance was dissolved in 100 ml of water again, 100 ml of barium chloride solution with a molar concentration of 1.1 was added, heated to boiling and stirred for 5 minutes, cooled to room temperature naturally, filtered with suction, and dried in an oven at 50 degrees to obtain 5,5'- Azotetrazole zinc salt.
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