Temperature-resistant and salt-resistant fluid loss reducer for drilling fluid and preparation method thereof
A fluid loss reducing agent, drilling fluid technology, applied in chemical instruments and methods, drilling composition and other directions, can solve the problems of destroying drilling fluid rheology and fluid loss, drilling fluid loss of efficacy, and bottom hole temperature rise. , to achieve the effect of stabilizing the wellbore, protecting the wellbore, and increasing the bonding ability
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
preparation example 1
[0032] A preparation method of water-based acrylic resin, comprising the following steps:
[0033] Wash the monomer styrene and butyl acrylate with 5wt% sodium hydroxide solution until colorless, then wash with distilled water until neutral, carry out oil-water separation, and then pass the washed monomer through anhydrous sulfuric acid Sodium sand core funnel to remove water;
[0034] In grams by weight, dissolve 280g of styrene after washing, 100g of butyl acrylate, 20g of acrylic acid and 5.5g of emulsifier in 100g of water to prepare a pre-emulsion, then add 0.2g of potassium persulfate, and add the above-mentioned potassium persulfate The pre-emulsion was added dropwise to 300g of water at 70°C, stirred, and reacted for 2.5 hours, then kept warm for 45 minutes and adjusted to a pH value of 8, then washed with ethanol and distilled water successively, dried, and crushed to obtain a water-based acrylic resin, wherein the emulsifier was Nonylphenol polyoxyethylene ether NP-...
preparation example 2
[0036] A kind of preparation method of water-based acrylic resin is carried out according to the method in Preparation Example 1, the difference is that
[0037] Wash the monomer styrene and butyl acrylate with 5wt% sodium hydroxide solution until colorless, then wash with distilled water until neutral, carry out oil-water separation, and then pass the washed monomer through anhydrous sulfuric acid Sodium sand core funnel to remove water;
[0038] In terms of g by weight, 250g of styrene after washing, 80g of butyl acrylate, 15g of acrylic acid and 5g of emulsifier were dissolved in 90g of water to prepare a pre-emulsion, and then 0.1g of potassium persulfate was added. Add the pre-emulsion dropwise to 280g water at 65°C, stir, react for 2 hours, then keep it warm for 0.5 hours and adjust the pH value to 8, then wash with ethanol and distilled water successively, dry, and pulverize to obtain a water-based acrylic resin, in which the emulsifier is mass Nonylphenol ethoxylate N...
preparation example 3
[0040] A preparation method of water-based acrylic resin, comprising the following steps:
[0041] Wash the monomer styrene and butyl acrylate with 5wt% sodium hydroxide solution until colorless, then wash with distilled water until neutral, carry out oil-water separation, and then pass the washed monomer through anhydrous sulfuric acid Sodium sand core funnel to remove water;
[0042] In grams by weight, 300g of styrene after washing, 120g of butyl acrylate, 25g of acrylic acid and 6g of emulsifier were dissolved in 120g of water to prepare a pre-emulsion, and then 0.3g of potassium persulfate was added. Add the pre-emulsion dropwise to 330g water at 75°C, stir, react for 3 hours, then keep it warm for 1 hour and adjust the pH value to 8, then wash with ethanol and distilled water successively, dry, and pulverize to obtain a water-based acrylic resin, wherein the emulsifier is the mass ratio It is 2:3 nonylphenol polyoxyethylene ether NP-10 and octylphenol polyoxyethylene et...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com