A kind of preparation method of superhydrophobic lipophilic material
A water-friendly and super-hydrophobic technology, which is applied in the field of preparation of super-hydrophobic and lipophilic materials, can solve problems such as uncontrollable infiltration uniformity, complex raw materials and ratios, and potential safety hazards, so as to improve hydrophobic and lipophilic properties and the effect of using persistence
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Embodiment 1
[0032] (1) Select a foamed nickel material with a void density of 110PPI and cut it into a sample of 5cm*5cm*0.3cm, wash it with anhydrous ethanol for 3 times, then with deionized water for 3 times, and ultrasonic vibration cleaning, each time for 10 minutes, at 50°C Dry down for later use;
[0033] (2) Weigh 0.25g of dopamine in 95ml of water, adjust the solution to pH 8.5 with 0.1M / L hydrochloric acid solution and Tris solution, add 5ml of graphene oxide aqueous solution with a concentration of 0.5mg / mL, and ultrasonically vibrate for 10min , under the condition of 25°C, magnetic stirring for 12h, vacuum filtration and drying at 75°C to obtain polydopamine-graphene oxide.
[0034] (3) Weigh 0.20g of dopamine in 100ml of water, adjust the solution to pH 8.5 with 0.1M / L hydrochloric acid solution and Tris solution, and add the polydopamine-graphene oxide obtained in step (2) into the prepared In the dopamine solution, ultrasound was applied for 20 minutes, and the prepared ni...
Embodiment 2
[0040] (1) Select a foam nickel material with a void density of 125PPI and cut it into a sample of 5cm*5cm*0.3cm, wash it 3 times with absolute ethanol, then wash it with deionized water 3 times, and clean it with ultrasonic vibration, each time for 10 minutes, at 50°C drying spare;
[0041] (2) Weigh 0.25g of dopamine in 93ml of water, adjust the solution to pH=8.5 with 0.1M / L hydrochloric acid solution and Tris solution, add 7ml of graphene oxide aqueous solution with a concentration of 0.5mg / mL, and ultrasonically vibrate for 15min , under the condition of 25° C., magnetic stirring for 11 h, vacuum filtration and drying at 65° C. to obtain polydopamine-graphene oxide.
[0042] (3) Weigh 0.20g of dopamine in 100ml of water, adjust the solution to pH=8.5 with 0.1M / L hydrochloric acid solution and Tris solution, and add the polydopamine-graphene oxide obtained in step (2) into the prepared In the dopamine solution, ultrasonically for 20 minutes, the prepared matrix material w...
Embodiment 3
[0048] (1) Select a titanium foam material with a void density of 130PPI and cut it into a sample of 5cm*5cm*0.3cm, wash it twice with anhydrous ethanol, then wash it twice with deionized water, and clean it with ultrasonic vibration, each time for 6 minutes, at 50°C drying spare;
[0049] (2) Weigh 0.18g of dopamine in 90ml of water, adjust the solution to pH=8.5 with 0.1M / L hydrochloric acid solution and Tris solution, add 10ml of graphene oxide aqueous solution with a concentration of 0.1mg / mL, and ultrasonically vibrate for 15min , under the condition of 25° C., magnetic stirring for 14 h, vacuum filtration and drying at 65° C. to obtain polydopamine-graphene oxide.
[0050] (3) Weigh 0.15g of dopamine in 100ml of water, adjust the solution to pH=8.5 with 0.1M / L hydrochloric acid solution and Tris solution, add the polydopamine-graphene oxide obtained in step (2) into the prepared In the dopamine solution, ultrasonic for 15 minutes, the prepared matrix material was immers...
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