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Heat-insulation ablation-resistant maintainable repairing agent and coating dual-purpose slurry, preparation method and application

A kind of anti-ablation and repairing agent technology, applied in the direction of coating, etc., can solve the problems of increasing cost, poor compatibility between coating and substrate, high coating density, etc., to improve heat resistance temperature and time, and avoid solvent volatilization loss , good heat insulation effect

Active Publication Date: 2020-02-21
BEIJING INSTITUTE OF TECHNOLOGYGY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] (1) The preparation process of the inorganic thermal protective coating requires high-temperature sintering, which leads to large residual thermal stress in the coating and makes it difficult to achieve large-area coating preparation;
[0005] (2) High cost;
[0006] (3) The coating density is high;
[0007] (4) The coating is brittle and the assembly process of the coated insulation tile is complex, easy to be damaged during assembly and service, and cannot be maintained;
[0008] (5) Poor compatibility between traditional coatings and substrates, etc.
[0009] Although organic high-temperature-resistant coatings are low in cost and have good compatibility with substrates, they need to be cured at high temperatures for a long time, the high-temperature residual carbon rate is low, and the heat-resistant temperature is below 600°C, which is difficult to meet the development needs of future reusable thermal protection systems.
At the same time, due to its greater brittleness and complex assembly process, the thermal protection system is easy to be damaged and unmaintainable due to bumps in the assembly process, which causes a great waste of resources and greatly increases the cost

Method used

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  • Heat-insulation ablation-resistant maintainable repairing agent and coating dual-purpose slurry, preparation method and application

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0041] A dual-purpose slurry for a heat-insulating, ablation-resistant, maintainable repair agent and a coating, the slurry is composed of a main component and an additional component, based on the total mass of the main component being 100%. The fractions are as follows: silicone resin 40%, high temperature resistant filler 60%; the composition and mass fraction of the added components are as follows: the mass fraction of the solvent is 60% of the mass of the main component; the mass fraction of the additive is the mass of the main component 1.5%.

[0042] The silicone resin is methylphenyl silicone resin.

[0043] The high temperature resistant filler is composed of boron carbide, titanium dioxide, kaolin, chopped mullite fiber, hollow glass microspheres and silica hollow microspheres in a mass ratio of 2:2:3:1:4:3.

[0044] The solvent is absolute ethanol.

[0045] The auxiliary agent is a mixed solution of silane coupling agents KH550 and KH-560, and the mass ratio of KH...

Embodiment 2

[0051] A dual-purpose slurry for a heat-insulating, ablation-resistant, maintainable repair agent and a coating, the slurry is composed of a main component and an additional component, based on the total mass of the main component being 100%. The fractions are as follows: silicone resin 40%, high temperature resistant filler 60%; the composition and mass fraction of the added components are as follows: the mass fraction of the solvent is 70% of the mass of the main component; the mass fraction of the additive is the mass of the main component 2.5%.

[0052] The silicone resin is a mixture of methyl silicone resin and phenyl silicone resin, and the mass ratio of methyl silicone resin and phenyl silicone resin is 2:1.

[0053]The high temperature resistant filler is composed of boron carbide, silicon powder, kaolin, boron trioxide and mica powder in a mass ratio of 2:1:3:1:3.

[0054] The solvent is a mixed solution of xylene and absolute ethanol, and the mass ratio of xylene t...

Embodiment 3

[0061] A dual-purpose slurry for a heat-insulating, ablation-resistant, maintainable repair agent and a coating, the slurry is composed of a main component and an additional component, based on the total mass of the main component being 100%. The fractions are as follows: silicone resin 50%, high temperature resistant filler 50%; the composition and mass fraction of the added components are as follows: the mass fraction of the solvent is 65% of the mass of the main component; the mass fraction of the additive is the mass of the main component 2%.

[0062] The silicone resin is a mixture of methyl silicone resin and phenyl silicone resin, and the mass ratio of methyl silicone resin and phenyl silicone resin is 1:1.

[0063] The high temperature resistant filler is composed of boron carbide, boron nitride, silicon dioxide, aluminum oxide and mica powder in a mass ratio of 1:1:3:2:3.

[0064] The solvent is a mixed solution of toluene and xylene, and the mass ratio of toluene to...

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Abstract

The invention relates to a heat-insulating ablation-resistant maintainable repairing agent, coating dual-purpose slurry, a preparation method and application, and belongs to the technical field of coatings and repairing agents. The slurry comprises main components and an additive component, the main components comprise 40-60% of organic silicon resin and 40-60% of a high-temperature-resistant filler the additive component comprises a solvent, wherein the mass of the solvent accounts for 60%-70% of the mass of the main components, and the additive component can further comprise an auxiliary agent; the main components and the additive component are uniformly mixed to obtain the slurry; the slurry is applied to gaps, pits, damage and other defects needing to be repaired, and repairing of a defect-containing base body is completed after curing. And by brushing the slurry on a matrix, and curing, the coating is obtained. The slurry can be used for preparing coatings and repairing defects onthe surfaces of various substrates, has the effects of heat insulation and ablation resistance, remarkably improves the temperature resistance of the substrates, and can meet the requirements of aircraft thermal protection systems in the future for low-cost, heat-proof, ablation-resistant and maintainable repairing agents and coatings.

Description

technical field [0001] The invention relates to a heat-insulating, ablation-resistant and maintainable repairing agent and a coating dual-purpose slurry, a preparation method and an application thereof, which can be used for repairing, leveling and caulking in the maintenance process of various substrates, and can also be directly used for preparing durable The invention relates to a high-temperature heat-insulating coating, which belongs to the technical field of coating and repairing agent. Background technique [0002] With the development of reusable hypersonic vehicle technology, the development of reusable thermal protection system is of great significance. Heat-insulating, ablation-resistant and maintainable high-temperature-resistant protective coating technology provides technical support for high-performance reusable thermal protection systems. [0003] Traditional high temperature resistant thermal protective coatings are divided into two categories: inorganic an...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09D183/04C09D7/61
CPCC08K2003/2227C08K2003/2241C08K2003/385C08K2201/014C08L2201/08C08L2205/025C09D183/04C09D7/61C09D7/70C08K13/04C08K7/28C08K7/26C08K7/10C08K3/38C08K3/22C08K3/346C08L83/04C08K13/02C08K3/36C08K3/34
Inventor 徐宝升周宁方岱宁钟政祥王一光杨亚政
Owner BEIJING INSTITUTE OF TECHNOLOGYGY
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