Reinforced and toughened polycarboxylate water reducer, preparation method and preparation device

A polycarboxylic acid-based, reinforced and toughened technology, applied in the direction of feeding devices, chemical instruments and methods, chemical/physical processes, etc., can solve the problem of water reducer product quality deterioration, accelerated polymer deterioration, and water reducer Poor work performance and other problems, to achieve the effect of convenient construction, saving reaction time, low water absorption

Active Publication Date: 2022-03-08
GUANGZHOU JIANSHENG BUILDING MATERIALS CO LTD
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Problems solved by technology

[0005] However, the existing polycarboxylate-based water-reducers are highly sensitive to temperature. When the temperature rises, the macromolecular chains in the product will move intensified, and chain decomposition and random fracture will easily occur, resulting in accelerated deterioration of the polymer. As a result, the quality of the water reducer product deteriorates. Therefore, at high temperatures, the performance of the polycarboxylate water reducer is poor and the slump retention is insufficient.

Method used

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  • Reinforced and toughened polycarboxylate water reducer, preparation method and preparation device
  • Reinforced and toughened polycarboxylate water reducer, preparation method and preparation device
  • Reinforced and toughened polycarboxylate water reducer, preparation method and preparation device

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Embodiment

[0052] see figure 1 , a method for preparing a reinforced and toughened polycarboxylate water reducer, comprising the following steps:

[0053] The first step, take by weight 20 parts of methacrylic acid, 15 parts of acrylic acid, 10 parts of ethyl acrylate, 10 parts of hydroxyethyl acrylate, 10 parts of sodium allyl sulfonate, 8 parts of methyl methacrylate, 5 parts of allyl polyoxyethylene ether, 0.5 parts of initiator, 3 parts of thermal storage porcelain powder, and 1 part of molecular weight regulator;

[0054] The second step: mix methacrylic acid, acrylic acid, ethyl acrylate, hydroxyethyl acrylate, sodium allyl sulfonate, methyl methacrylate, allyl polyoxyethylene ether, molecular weight regulator and deionized water, Making a polymerized monomer solution with a content of 50% by mass percentage;

[0055] The third step: the initiator is mixed with water to make an initiator solution with a content of 10% by mass percentage;

[0056] The initiator is selected from o...

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Abstract

The invention discloses a reinforced and toughened polycarboxylate water reducer, a preparation method and a preparation device, and belongs to the technical field of polycarboxylate water reducer preparation. Add initiator solution and thermal storage ceramic powder to keep the same adding time, save the reaction time and at the same time make the materials mixed more fully and evenly, and improve the preparation efficiency of polycarboxylate water reducer; when the external temperature When it rises, the thermal storage porcelain powder will absorb a large amount of heat, so that the molecular chains in the polycarboxylate superplasticizer cannot absorb enough heat to decompose and break, maintain their original molecular properties, improve thermal stability, and significantly It improves its slump retention performance at high temperature; at the same time, due to the extremely low water absorption rate of heat storage porcelain powder, it reduces the HLB (water oil degree) value, reduces the possibility of cement particles and water forming bound water, and releases more Free water, thereby reducing cement paste viscosity.

Description

technical field [0001] The invention relates to the technical field of preparation of polycarboxylate water-reducer, more specifically, to a reinforced and toughened polycarboxylate water-reducer, a preparation method and a preparation device. Background technique [0002] In recent years, my country's infrastructure such as high-speed rail, highways, airports, dams, and municipal engineering has maintained rapid growth, and it has also promoted the rapid development of concrete admixture technology. The development of concrete admixtures can be roughly divided into the following stages: the first stage is the initial stage, represented by ordinary water reducer lignin; the second stage is the development stage represented by naphthalene-based superplasticizers, melamine, Sulfamate-based, aliphatic water-reducing agents and other water-reducing agents; the third stage is the current stage, which is the stage when concrete admixtures are moving towards the high-tech field, wi...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B18/02C04B24/16C08F283/06C08F220/06C08F220/18C08F220/20C08F228/02C08F220/14B01J4/02B01J19/00C04B103/30
CPCC04B18/023C04B40/0046C08F283/065B01J4/02B01J19/0053C04B2103/302C04B14/303C04B14/06C04B14/304C04B14/30C04B14/106C04B14/305C04B14/041C04B24/165C08F220/06C08F220/20C08F228/02C08F220/14
Inventor 卢伟雄肖山虎蔡健
Owner GUANGZHOU JIANSHENG BUILDING MATERIALS CO LTD
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