Oral drug-loaded patch film and preparation method thereof, and oral drug-loaded patch film assembly and preparation method thereof
A technology of drug loading and oral cavity, which is applied in drug combination, pharmaceutical formula, drug delivery, etc., can solve the problems of thick thickness, easy to fall off, and barrier effect to reduce the effective absorption of drugs, so as to achieve the effect of improving the therapeutic effect and not easy to fall off
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[0068] The embodiment of the present invention also provides a preparation method of the above-mentioned oral drug-loaded patch, comprising the following steps:
[0069] Loading the drug-loaded particles on the carrier film, specifically, the loading step includes: mixing the first solution containing the drug-loaded particles with the second solution containing a dopa-modified polymer, Then freeze-dry to form the carrier film, and the drug-loaded particles are loaded on the carrier film. The above operation steps can ensure the formation of oral drug-loaded film.
[0070] Wherein, the preparation step of the first solution includes: mixing and dissolving the coating material and the active ingredient, then adding it to a poor solvent, stirring and mixing, and then centrifuging to form a centrifugal sediment; at this time, the coating material has wrapped the active ingredient, so that the active ingredient Can be sustained slow release.
[0071] Further, both the coating ma...
Embodiment 1
[0082] The present embodiment provides a preparation method of an oral drug-loaded patch, comprising the following steps:
[0083] S1, preparing the first solution;
[0084] Dissolve 40mg of polylactic-co-glycolic acid (PLGA) and 4mg of dexamethasone (Dex) in 2ml of acetonitrile solution, then slowly drop into 40ml of deionized water, stir and react at 25°C for 4 hours, and then centrifuge at 12000rpm for 20min at high speed to form sink, and washed repeatedly three times to form a centrifugal sediment.
[0085] In 40ml of deionized water, tris (Tris) was added to make the pH of the solution 10, and then 0.5mg of dopamine hydrochloride (C 8 h 11 NO 2 HCl), stir until it is completely dissolved, add the aforementioned centrifugal sediment and let it dissolve, then, stir and react at 25°C for 6h, then centrifuge at 12000rpm for 20min to collect the sediment after centrifugation, and wash the sediment several times , forming a first solution, the first solution contains PLGA-...
Embodiment 2
[0094] Example 2 When preparing the second solution, 4 mmol of 3,4-dihydroxyphenylalanine (DOPA) was added, and the number of the polymer modified by the dopa-like substance formed was PVA-DOPA2;
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