Sea cucumber polysaccharide composition as well as preparation method and application thereof
A sea cucumber polysaccharide and composition technology, applied in the field of medicine, can solve the problems of limited use effect and single strain
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Embodiment 1
[0035] A sea cucumber polysaccharide composition is prepared from the following raw materials in parts by weight: 200 g of sea cucumber, 100 g of mulberry leaves, 100 g of purslane, 50 g of gallinaceous gold and 50 g of malt; the preparation method comprises the following steps:
[0036]S1: Preparation of sea cucumber polysaccharide extract: Weigh sea cucumber, mulberry leaves and purslane according to weight ratio, mix them evenly and crush them into 300 meshes, add 8 times the mass of pure water at 80°C to extract 3 times, cool to room temperature Centrifuge at a speed of 3000r / min, discard the centrifuge and precipitate to obtain the supernatant, concentrate the supernatant at 60°C, add 5 times the mass of 80v / v% ethanol aqueous solution for precipitation, let stand for 48h, collect the precipitate and use Sephdex LH- 20 gel column chromatography for separation, followed by eluting with 20v / v%, 30v / v%, and 40v / v% methanol aqueous solution, combining the eluents and freeze-dr...
Embodiment 2
[0038] A sea cucumber polysaccharide composition is prepared from the following raw materials in parts by weight: 400 g of sea cucumber, 200 g of mulberry leaves, 200 g of purslane, 150 g of gallinaceous gold and 150 g of malt; the preparation method comprises the following steps:
[0039] S1: Preparation of sea cucumber polysaccharide extract: Weigh sea cucumber, mulberry leaf and purslane according to weight ratio, mix them evenly and crush them into 100 mesh, add 3 times the mass of pure water at 60°C for extraction once, cool to room temperature Centrifuge at a speed of 1000r / min, discard the centrifuge and precipitate to obtain the supernatant, after the supernatant is concentrated at 40°C, add 3 times its mass of 60v / v% ethanol aqueous solution for precipitation, let it stand for 24h, collect the precipitate and use Sephdex LH- 20 gel column chromatography for separation, followed by eluting with 20v / v%, 30v / v%, and 40v / v% methanol aqueous solution, combining the eluents ...
Embodiment 3
[0041] A sea cucumber polysaccharide composition is prepared from the following raw materials in parts by weight: 240g sea cucumber, 120g mulberry leaves, 120g purslane, 80g gallinaceous gold and 80g malt; the preparation method comprises the following steps:
[0042] S1: Preparation of sea cucumber polysaccharide extract: Weigh sea cucumber, mulberry leaves and purslane according to weight ratio, mix them evenly and crush them into 200 meshes, add 6 times the mass of pure water at 75°C for extraction twice, and cool to room temperature Centrifuge at a speed of 1500r / min, discard the centrifuge and precipitate to obtain the supernatant, concentrate the supernatant at 50°C, add 4.5 times the mass of 70v / v% ethanol aqueous solution for precipitation, let stand for 36h, collect the precipitate and use Sephdex LH- 20 gel column chromatography for separation, followed by eluting with 20v / v%, 30v / v%, and 40v / v% methanol aqueous solution, combining the eluents and freeze-drying to obt...
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