Preparation method of 3D printing acrylic reinforced bathtub material
A technology for printing acrylic and reinforced materials, applied in the direction of additive processing, etc., can solve the problems of coating wear, non-wear-resistant surface, easy aging and discoloration, etc., and achieve the effect of improving heat resistance, good heat resistance and smooth hand feeling
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Embodiment 1
[0023](1) Dehydrate the polymer polyol and dimethylol butyric acid at 105°C and a vacuum of 0.08 MPa for 2 hours, remove the polymerization inhibitor from the methyl methacrylate and re-steam, set aside, diisocyanate, polymer polyol and Add 2-methyl-2,4-pentanediol in a molar ratio of 5:2:1 to a reaction kettle equipped with a mechanical stirrer and a condenser tube, and add methyl methacrylate 0.8 times the weight of the polymer polyol The ester was used as a solvent, and the reaction was stirred at 50°C for 2h; (2) at 70°C, the ratio by weight (N-methylpyrrolidone) : dimethylol butyric acid = 3:1, adding the N-methylol butyric acid Methylpyrrolidone solution, then add methyl methacrylate 0.6 times the weight of dimethylol butyric acid, and react for 3 hours; (3) Lower the temperature to 40°C, then add methacrylic acid 0.4 times the weight of dimethylol butyric acid Methyl ester, according to the ratio of substances, the amount of dimethylol butyric acid: catalyst = 1: 1 is a...
Embodiment 2
[0025] (1) Dehydrate the polymer polyol and dimethylol butyric acid at 105°C and a vacuum of 0.08 MPa for 2 hours, remove the polymerization inhibitor from the methyl methacrylate and re-steam, set aside, diisocyanate, polymer polyol and Add 2-methyl-2,4-pentanediol in a molar ratio of 4:1:1 to a reaction kettle equipped with a mechanical stirrer and a condenser tube, and add methyl methacrylate 0.6 times the weight of the polymer polyol The ester was used as a solvent, and the reaction was stirred at 50°C for 1h; (2) at 70°C, by weight, N-methylpyrrolidone: dimethylolbutyric acid = 3:1, adding N-methylolbutyric acid Methylpyrrolidone solution, then add methyl methacrylate 0.4 times the weight of dimethylol butyric acid, and react for 2 hours; (3) Lower the temperature to 40°C, then add methacrylic acid 0.2 times the weight of dimethylol butyric acid Methyl ester, according to the ratio of substances, the amount of dimethylol butyric acid:catalyst=1:1 is then added to the cata...
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