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Preparation method of graphene-polyester nanometer composite fiber

A nanocomposite fiber and graphene technology, applied in fiber processing, fiber chemical characteristics, melt spinning, etc., can solve problems such as uneven fiber texture, different drawing time, and unstable spinning quality, and achieve high spinning quality High, uniform cooling effect, improve the effect of uniform cooling effect

Inactive Publication Date: 2020-09-22
孟伟东
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] In order to make up for the deficiencies of the existing technology and solve the problem in the prior art, after the melt is spun from the spinneret, it releases a large amount of solidification heat into the surrounding air. Therefore, it is necessary to blow cold air to carry out convective heat after the solidified filament is passed out of the spinneret. Exchange, to take away the released heat to solidify the melt stream into fibers. In the cooling process, uniform air supply is very important. Uneven side blowing air supply will cause uneven fiber dryness. At the same time, side blowing and ring blowing Because the wind direction is perpendicular to the fiber, the uneven wind speed will easily lead to air turbulence, causing the problem of floating yarn to rise, and then the raw fiber is uneven, which makes the drawing time different, and the fiber diameter is different, which leads to spinning. Unstable silk quality and other issues, the present invention proposes a preparation method of graphene-polyester nanocomposite fibers

Method used

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preparation example Construction

[0028] Such as Figure 1 to Figure 5 Shown, the preparation method of a kind of graphene-polyester nanocomposite fiber of the present invention, this preparation method comprises the following steps:

[0029] S1: The polyester polyester chips need to be dried before use, and at the same time, the graphene is peeled off by mechanical ball milling, and the dried polyester polyester chips and the peeled graphene are mixed according to the mass ratio of 100:0.1~20 to obtain a mixture , and introduce the mixture into the stirring tank; graphene, as a two-dimensional honeycomb crystal composed of carbon atoms, has unparalleled mechanical properties and functionalities such as electrical conductivity, thermal conductivity, antibacterial, and radiation resistance. It is currently the thinnest known , the material with the highest strength, so compared with the prior art, the breaking strength of the graphene-polyester nanocomposite fiber has been greatly improved;

[0030] S2: Set th...

Embodiment approach

[0034] As an embodiment of the present invention, the front and rear longitudinal sections of the air guide rod 3 are designed with a triangular structure; the opposite sides of the air guide rod 3 are designed with a tapered structure; The cross-section of the rod 3 is designed as a triangular structure. When the spinning fiber is pulled down and passes through the air guide rod 3, it can be pulled more smoothly, reducing the resistance effect of the air guide rod 3 on the downward pulling of the spinning fiber, and avoiding air guide The rod 3 causes a large area of ​​broken filaments in the spinning fiber. At the same time, the end surface of the air guide rod 3 is designed as a tapered structure. fibers, causing breakage of the spun fibers.

[0035] As an embodiment of the present invention, the left and right sides of the box body 1 are fixedly connected with fixing blocks 33 at the position of the cold plate 31; Both are provided with chute, and the cold plate 31 is all...

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Abstract

The invention belongs to the technical field of composite fibers and specifically relates to a preparation method of a graphene-polyester nanometer composite fiber. A spinning box used in the preparation method of the graphene-polyester nanometer composite fiber is provided with a box body, a rotating disc and an air guide rod; a spinneret plate is arranged in a position, close to the upper surface of the box body, in the box body; a conduit is fixedly connected to the lower surface of the spinneret plate; a cold plate is fixedly connected to the position, close to the lower end surface of theconduit, in the box body; the air guide rod is connected to the interior of the cold plate to slide from left to right; and the rotating disc is rotationally connected to the interior of the conduit.Through adoption of the preparation method of the graphene-polyester nanometer composite fiber, parallel airflow cooling of spun fibers is effectively realized, the wind direction and the fibers areprevented from being in a vertical state, uneven air speed is very easy to cause air turbulence to cause a filament drifting problem, and meanwhile, the cooling effect on the spun fibers is more uniform so that the cooling time of the spun fibers and the drawing ratio are kept consistent with each other; and therefore, the qualities of the prepared spun silks are higher.

Description

technical field [0001] The invention belongs to the technical field of composite fiber production, in particular to a preparation method of graphene-polyester nano composite fiber. Background technique [0002] Graphene is the thinnest two-dimensional nanomaterial known so far. Its lattice is a hexagonal 2 shape surrounded by six carbon atoms, with a thickness of one atomic layer. The carbon atoms are connected by s-bonds. sp hybridization, these s bonds endow graphene with extremely excellent mechanical properties and structural rigidity. The strength of graphene is 100 times stronger than the best steel. Graphene has high conductivity and is the smallest resistivity in the world. Material; graphene is also a very good antibacterial material, based on the mechanical properties of graphene, graphene can be added to the polymer matrix, which can improve the mechanical properties of the material, such as tensile strength, modulus, hardness etc.; based on the excellent electri...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D01D5/092D01D5/08D01D4/00D01F6/92D01F1/10
CPCD01D4/00D01D5/08D01D5/092D01F1/10D01F6/92
Inventor 孟伟东周乾松沈斌
Owner 孟伟东
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