Methyl bromide impurity removal process adopting strong base
A technology of methyl bromide and process, which is applied in the field of impurity removal process of methyl bromide using strong alkali, can solve the problems of cumbersome operation, low purity of methyl bromide, high energy consumption, etc., and achieve the effect of improving purity, reducing energy consumption, and thoroughly removing impurities
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Embodiment 1
[0029] A kind of methyl bromide impurity removal process that adopts strong alkali comprises the following steps:
[0030] (1) Neutralization treatment: Methyl bromide gas is passed into the first absorption tower from the bottom of the first absorption tower at a ventilation rate of 240m³ / h, and discharged from the top of the first absorption tower; hydrogen with a mass concentration of 15% Sodium oxide solution is sprayed from the top of the first absorption tower with a spray rate of 1m³ / h, and discharged from the bottom of the first absorption tower; wherein, the height of the packing layer is 2m; the temperature at which methyl bromide passes into the first absorption tower is 20 ℃, the temperature of sodium hydroxide solution spraying is 20 ℃, and the tower internal pressure of the first absorption tower is 90kPa.
[0031] (2) Drying treatment: the methyl bromide discharged in the step (1) is passed into the second absorption tower from the bottom of the second absorptio...
Embodiment 2
[0034] A kind of methyl bromide impurity removal process that adopts strong alkali comprises the following steps:
[0035] (1) Neutralization treatment: Methyl bromide gas is passed into the first absorption tower from the bottom of the first absorption tower at a ventilation rate of 243m³ / h, and discharged from the top of the first absorption tower; hydrogen with a mass concentration of 20% Sodium oxide solution is sprayed from the top of the first absorption tower with a spray rate of 1.3m³ / h, and discharged from the bottom of the first absorption tower; wherein, the height of the packing layer is 2.8m; the temperature at which methyl bromide passes into the first absorption tower The temperature is 25°C, the temperature of sodium hydroxide solution spraying is 30°C, and the pressure inside the first absorption tower is 100kPa.
[0036] (2) Drying treatment: the methyl bromide discharged in the step (1) is passed into the second absorption tower from the bottom of the second...
Embodiment 3
[0039] A kind of methyl bromide impurity removal process that adopts strong alkali comprises the following steps:
[0040] (1) Neutralization treatment: Methyl bromide gas is passed into the first absorption tower from the bottom of the first absorption tower at a ventilation rate of 246m³ / h, and discharged from the top of the first absorption tower; hydrogen with a mass concentration of 21% Sodium oxide solution is sprayed from the top of the first absorption tower with a spray rate of 1.6m³ / h, and discharged from the bottom of the first absorption tower; wherein, the height of the packing layer is 3.5m; the temperature at which methyl bromide is passed into the first absorption tower is 30°C, the temperature of sodium hydroxide solution spraying is 35°C, and the pressure inside the first absorption tower is 110kPa.
[0041] (2) Drying treatment: the methyl bromide discharged in step (1) is passed into the second absorption tower from the bottom of the second absorption tower...
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