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316results about How to "Reduce decomposition rate" patented technology

Composite flame retardant containing microcapsule-coated intumescent flame retardant and preparation method

The invention belongs to the field of flame retardant materials, and particularly relates to a composite flame retardant containing a microcapsule-coated intumescent flame retardant and a preparation method. The composite flame retardant containing the microcapsule-coated intumescent flame retardant consists of the following components in percentage by mass: 60-94 percent of microcapsule intumescent flame retardant, 5-25 percent of flame-retardant synergist, 0.9-10 percent of smoke suppressant and 0.1-5 percent of hindered amine light stabilizer. The preparation method comprises the following steps: preparing the microcapsule-coated intumescent flame retardant; placing the microcapsule-coated intumescent flame retardant, the flame-retardant synergist, the smoke suppressant and the hindered amine light stabilizer into a high-speed mixer for mixing uniformly, and discharging to obtain the composite flame retardant containing the microcapsule-coated intumescent flame retardant. Multiple components in the composite flame retardant can play roles in retarding flame in a synergetic way, so that the flame retardance of a high polymer material is improved remarkably, the production of toxic and harmful smog in a burning process can be suppressed, and the flame retarding efficiency is increased greatly.
Owner:LIAONING TECHNICAL UNIVERSITY

Preparation method of microencapsulated gradient halogen-free flame retardant system

The invention relates to a preparation method of a microencapsulated gradient halogen-free flame retardant system. The preparation method comprises the steps of: mixing a phosphorus-series flame retardant with an inorganic flame retardant according to a certain ratio to obtain a microencapsulated halogen-free flame retardant, then carrying out surface modification on a charring agent, and then mixing the microencapsulated halogen-free flame retardant, a phosphorus-containing organic flame retardant and surface-modified charring agent according to a certain ratio to obtain the microencapsulated gradient halogen-free flame retardant system. By using the system, distributed gradient flame retarding is realized, the flame retardancy of a polymer material is greatly improved, the defect that compatibility between the flame retardant and the polymer is poor is solved, the migration of the halogen-free flame retardant from the polymer matrix under high-temperature and moisture conditions is significantly reduced, and the long-term storage of a flame-retardant polymer material is facilitated. The method has the characteristics of simple process, convenience for operation, environmental friendliness, and lower cost. The obtained flame retardant system has good flame retarding effect and wide application field.
Owner:JILIN UNIV

Method for preparing brake block by calcium carbonate crystal whisker

The invention relates to a method for preparing a brake sheet through adopting calcium carbonate crystal whisker, belonging to the friction material field, wherein the following raw materials of corresponding part by weight are adopted: 5 to 15 portions of adhesive which adopts phenol formaldehyde resin, 20 to 30 portions of reinforcing material which is obtained through mixing steel fiber or ceramic fiber with one or several of aramid fiber, mineral fiber and glass fiber, 1 to 15 portions of grinding agent which comprises one or combination of several of aluminum sesquioxide, ferric oxide, magnesium oxide and friction powder, 5 to 15 portions of lubricant which comprises one or combination of several of graphite, molybdenum disulfide and mica, 5 to 15 portions of stabilizer calcium carbonate crystal whisker, and 30 to 50 portions of filler which comprises one or combination of several of barium sulfate, potassium titanate and magnesium oxide. The brake sheet, which is made through the method, can effectively increase porosity and improve the high-temperature resistance of material, thereby lowering the decomposition rate of organic material at a high temperature; meanwhile, the brake sheet can slow down the gaseous escape speed on a friction surface during fading, thereby reducing fading rate and the change rate of friction coefficient at high speed to less than 10 percent.
Owner:信义集团公司

Method for producing sodium hydrogen carbonate and ammonium sulfate by using sodium sulfate solution

The invention relates to a method for producing sodium hydrogen carbonate and ammonium sulfate by using a sodium sulfate solution, and belongs to the technical field of chemical engineering. The method comprises the following steps: a, absorbing circulating gas by using the sodium sulfate solution at -5 to 10 DEG C to obtain absorbing liquid; b, mixing the absorbing liquid, ammonium hydrogen carbonate and/or mixed salt at -5 to 20 DEG C to obtain mixed slurry; c, performing sealed reaction on the mixed slurry to obtain sodium hydrogen carbonate and reaction mother liquid; d, mixing the reaction mother liquid and complex salt to obtain salt mixture and primary frozen mother liquid after freezing; e, distilling the primary frozen mother liquid to obtain carbon dioxide, ammonium circulating gas and ammonium steaming mother liquid; f, adjusting the ammonium steaming mother liquid by acid to obtain an acidified solution and gas; g, mixing and freezing the acidified solution and crystallizedmother liquid to obtain complex salt and secondary frozen mother liquid; and h, evaporating and concentrating the secondary frozen mother liquid to separate out ammonium sulfate. The method is low inenvironmental pollution and high in raw material utilization rate.
Owner:SICHUAN UNIV

High-efficiency cyhalothrin microcapsule suspension and preparation method thereof

InactiveCN105076188AMeet the anti-efficacy requirementsReduce decompositionBiocideAnimal repellantsNon target organismControlled release
The invention relates to a microcapsule suspension, the high-efficiency cyhalothrin microcapsule suspension comprises the following components: 1-20% of high-efficiency cyhalothrin, 1-10% of a solvent, 1-8% of a capsule wall material, 0.1-3% of a protecting adhesive, 2-5% of an emulsifier, 3-5% of a dispersant, 0.01-14% of an adjuvant and 1-99% of water. The preparation method is characterized in that a high-efficiency cyhalothrin active substrate is taken as the capsule core, a polyurea resin is taken as the capsule wall material, an interfacial polymerization technology is used for preparing the high-efficiency cyhalothrin microcapsule suspension, and finally the cyhalothrin microcapsule suspension is prepared. The effective components in the cyhalothrin microcapsule suspension are concentrated in the capsule core, and other medium can be water, such that environmental pollution is reduced, and production cost is effectively reduced. The high-efficiency cyhalothrin microcapsule suspension has release controlling capability, pesticide lasting period can be prolonged by 3-10 times, acute toxicity of original medicine can be reduced, toxicity of the cyhalothrin microcapsule suspension on non-target organisms is also reduced, and the high-efficiency cyhalothrin microcapsule suspension is safe to use and transport.
Owner:南通联农佳田作物科技有限公司

Potassium humate compound fertilizer and preparation method thereof

The invention belongs to the field of a fertilizer, in particular to a potassium humate compound fertilizer and a preparation method thereof. The potassium humate compound fertilizer is prepared by mixing urea, potassium humate, monoammonium phosphate, ammonium chloride, calcium powder and bentonite with magnesium sulfate, zinc sulfate and medium / trace elements. The potassium humate compound fertilizer granulated by using a steam drum physical agglomeration method and the preparation method of the compound fertilizer have the advantages that the prepared potassium humate compound fertilizer has large particle size and high strength and does not agglomerate; the capabilities of water and fertility retention, heat preservation and ventilation of the soil are enhanced; the soil structure is improved; the soil fertility is increased; the problems of reduced soil fertility, environmental pollution, soil hardening, nutrition unbalance and stress resistance of crops are solved; the utilization rate of the fertilizer is improved; the defects of low fertilizer efficiency, insufficient nutrition utilization, overproof pesticide residue, severe nitrate accumulation and heavy metal pollution are overcome; the sustained-release effect against pesticide is realized; the agroecological environment is protected; and the efficiency, yield and crop quality are improved.
Owner:李林

Method for efficiently and recyclably synthesizing 2,4,6-trimethylbenzoyldiphenyl phosphine oxide

The invention discloses a method for efficiently and recyclably synthesizing 2,4,6-trimethylbenzoyldiphenyl phosphine oxide. The method comprises the following steps of a, selecting a vanadium source and a molecular sieve as reaction raw materials to prepare a vanadium molecular sieve catalyst; b, adding 2,4,6-trimethylbenzaldehyde and diphenyl phosphine oxide into a three-opening bottle in which dichloromethane is contained, and stirring at normal temperature to react for 6 hours; c, cooling the three-opening bottle in a low-temperature water bath to 8 to 10 DEG C, sequentially adding the vanadium molecular sieve catalyst and tert-butyl hydroperoxide into the three-opening bottle, stirring to react for 0.5 hour, and continuously stirring at normal temperature for 3 to 5 hours to obtain reaction liquid; and d, filtering the reaction liquid, recycling a vanadium molecular sieve, treating the obtained filtrate by aqueous solution of sodium thiosulfate to remove unreacted oxide, and performing post treatment to obtain a TPO (2,4,6-trimethylbenzoyldiphenyl phosphine oxide) product. As the vanadium molecular sieve serves as the catalyst and is matched with the tert-butyl hydroperoxide to prepare the TPO, the yield of the target product is increased, and the catalyst is environment friendly and recyclable.
Owner:SHANDONG UNIV OF SCI & TECH

Method for recovering potassium nitrate from anthraquinone dye alkali wastewater

The invention relates to a method for recovering potassium nitrate from anthraquinone dye alkali wastewater and belongs to the technical field of recovery and recycle of printing and dyeing wastewater. The method comprises the following steps of adding nitric acid into collected alkali wastewater, carrying out primary acidification with stirring for primary acidification time of 0.5-12h, when a solution pH value is in a range of 1-4, adding an adsorbent, a neutral flocculating agent or an acidic flocculating agent into the solution so that a precipitation reaction occurs, filtering the reaction product, adding nitric acid into the solution, carrying out secondary acidification with stirring for secondary acidification time of 0-8h, when a solution pH value is in a range of 3-5h, adding an adsorbent, a neutral flocculating agent or an acidic flocculating agent into the solution so that a precipitation reaction occurs, filtering the reaction product, and carrying out HNO3 oxidation, decoloring, condensation and salt-leaching so that a qualified industrial salt is obtained. The method is used for anthraquinone dye alkali wastewater, can realize recovery of a large amount of potassium nitrate, can remove organic matters in wastewater, can reduce a COD value of the wastewater, and can recover and recycle potassium nitrate.
Owner:ZHEJIANG QICAI ECO TECH CO LTD
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