Chlorpyrifos microcapsule suspension and preparation method thereof
A technology of microcapsule suspension and methapon, which is applied in the direction of botany equipment and methods, insecticides, biocides, etc., can solve the problems of polluting the environment, adverse health effects of users, waste of industrial resources, etc., and achieve skin irritation Reduction of sexual substances, reduction of application times, and reduction of toxicity levels
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Embodiment 1
[0065]
[0066]
[0067] The former medicine (97%) of 20g of trimephos is dissolved in 15g of xylene (commercially available material), then add 4g of toluene diisocyanate TDI (such as the product of Cangzhou Dahua TDI Co., Ltd.) and stir (oil phase) ; Add 2.0g of emulsifier fatty alcohol polyoxyethylene ether AEO-9 (such as the product of Nanjing Taihua Co., Ltd.), 10g of 10% polyvinyl alcohol PVA aqueous solution into 27.9g of deionized water and stir (water phase); Put the prepared oil phase into the water phase and turn on the high-speed homogenization to form a stable O / W emulsion. The average particle size of the emulsion is measured to be 2.65 μm; turn on the stirring (maintain 600 rpm), and then put the homogenized emulsion Be warming up to 75 ℃, slowly add the hexamethylenediamine of 0.4g simultaneously, maintain the solidification temperature of capsule wall material for 3 hours, add the xanthan gum (2 %) aqueous solution, 0.1g of glacial acetic acid to adjust ...
Embodiment 2
[0069]
[0070]
[0071] The former medicine of 32g of trimethaphos is dissolved in 15g of C9 aromatics solvent naphtha (such as the product of Jinling Petrochemical Co., Ltd.), then add 3g of polyphenyl polymethylene polyisocyanate PAPI (such as the product of Bayer, Germany) Stir with 2g of diphenylmethane diisocyanate MDI (such as the product of Yantai Wanhua Polyurethane Co., Ltd.) to be an oil phase; Gum Arabic (5%) aqueous solution was added to 19g of deionized water and stirred to form a water phase; put the configured oil phase into the water phase and turn on high-speed homogenization to form a stable O / W emulsion, and measure the average particle size of the emulsion 10.58 μm; start stirring (maintain 700 rpm), then raise the temperature of the homogenized emulsion to 50°C, and slowly add 0.4g of triethanolamine to maintain a stable solidification temperature of the capsule wall material for 8 hours, then add 3g of phosphoric acid Ester dispersant NP-P (such as...
Embodiment 3
[0073]
[0074]
[0075] The former medicine (97%) of 40g of trimephos is thermally dissolved in the xylene of 8g, then adds the polyphenyl polymethylene polyisocyanate PAPI of 5g (for example the product of German Bayer company) and the toluene diisocyanate of 0.9g TDI (such as the product of Cangzhou Dahua TDI Co., Ltd.) is stirred evenly to be an oil phase; 2.0 g of emulsifier NP-10 (such as the product of Nanjing Taihua Co., Ltd.), 5 g of xanthan gum (2%) aqueous solution are added Stir 32g of deionized water into the water phase; put the prepared oil phase into the water phase and turn on high-speed homogenization to form a stable O / W emulsion. The average particle size of the emulsion is measured to be 45.2 μm; turn on the stirring (maintain 800 rpm / min), then the homogenized emulsion was warmed up to 35°C, and at the same time, 0.6g of diethylenetriamine was slowly added to maintain a stable solidification temperature of the capsule wall material for 22 hours, and...
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