Magneto-rheological material, preparation method and iron container repairing method
A magneto-rheological and ferrous technology, applied in magnetic materials, inductance/transformer/magnet manufacturing, magnetic objects, etc., can solve problems such as poisoning, affecting production efficiency, gas or liquid leakage, etc.
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[0039] Based on the same inventive concept, an embodiment of the present invention also provides a method for preparing a magnetorheological material as described in any of the previous technical solutions, including:
[0040] S100, reacting the metal powder and the coupling agent in an acidic environment at 40-50°C for 1-3 hours to obtain a modified metal powder;
[0041] S200, reacting the resin, dispersant and modified metal powder at 45-65°C for 1-2 hours to obtain a magnetic fluid;
[0042] S300, adding a curing agent and a diluent to the obtained magnetic fluid, and reacting for 1-3 hours to obtain a magnetorheological material.
[0043] In step S100, the metal powder is dispersed in a solvent, and the acidic environment is passed through acetic acid. The solvent may be ethanol solution, and the concentration of the ethanol solution may be 85-99%. The pH of the solution may be 3-5.
[0044] The metal powder can be fully dispersed by mechanical stirring.
[0045] Afte...
Embodiment 1
[0065] Weigh 50g of micron-sized iron powder and add it to 50ml of 95% ethanol solution, add acetic acid to adjust the pH value to 4, ultrasonically disperse at 40°C and mechanically stir for 5 minutes, then gradually add 1.1ml of coupling agent to the system, After the dropwise addition, continue to ultrasonically disperse and react with mechanical stirring for 2 hours. After the reaction, the powder was filtered out and dried at 70°C until constant weight. Grind and disperse the dried powder, add 60g of epoxy resin, raise the temperature to 60°C, add 0.08g of fatty alcohol polyoxyethylene ether, and stir thoroughly for 1 hour. Add 30g polyamide, 0.4gDMP-30, 8g polyethylene polyamine, 0.1g monododecyl potassium phosphate, 0.1g sodium dodecylsulfonate to the system, mechanically stir for 1 hour at room temperature, and gradually Add 10 g of ethylene glycol diglycidyl ether to obtain a magnetorheological repair material, and finally test related properties.
Embodiment 2
[0067] Weigh 50g of micron-sized iron powder and add it to 50ml of 95% ethanol solution, add acetic acid to adjust the pH value to 4, ultrasonically disperse at 40°C and mechanically stir for 5 minutes, then gradually add 1.1ml of coupling agent to the system, After the dropwise addition, continue to ultrasonically disperse and react with mechanical stirring for 2 hours. After the reaction, the powder was filtered out and dried at 70°C until constant weight. Grind and disperse the dried powder, add 80g of epoxy resin, raise the temperature to 60°C, add 0.1g of fatty alcohol polyoxyethylene ether, and stir thoroughly for 1 hour. Add 60g polyamide, 1gDMP-30, 20g polyethylene polyamine, 0.1g monododecyl potassium phosphate, 0.1g sodium dodecylsulfonate to the system, mechanically stir for 1 hour at room temperature, and gradually add 20g of ethylene glycol diglycidyl ether was used to obtain the magnetorheological repair material, and the relevant properties were finally tested....
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