Nitrogen-doped phosphorene quantum dot and preparation method thereof
A nitrogen-doped, quantum dot technology, applied in the field of phosphorene quantum dots, can solve the problems of easy agglomeration and difficult dispersion of materials, and achieve the effects of easy dispersion, high water solubility, and avoidance of agglomeration
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Embodiment 1
[0039] (1) Preparation of nitrogen-doped black phosphorus material:
[0040] Blend 10g of red phosphorus, 2g of dicyandiamide, and 1g of tin iodide evenly, place them in a tubular muffle furnace, pass in argon as a protective gas, and increase the temperature of the furnace body at a heating rate of 1.5°C / min. Raised to 600 ° C, and constant temperature reaction for 3h. Then, the heating is stopped, and the furnace body is naturally lowered to room temperature, and the reaction product nitrogen-doped black phosphorus material is taken out.
[0041] (2) Preparation of nitrogen-doped phosphorene quantum dot materials:
[0042] Grind the nitrogen-doped black phosphorus material prepared in (1), and screen the powder with a particle size of 200 mesh, weigh 1g and place it in a 200mL beaker, add 100mL N-methylpyrrolidone as the dispersion medium, 0.1 g of europium trifluoromethanesulfonate was used as a stabilizer to obtain a mixed solution. The mixed solution was placed in an u...
Embodiment 2
[0046] (1) Preparation of nitrogen-doped black phosphorus material:
[0047] Blend 10g of red phosphorus, 2g of melamine, and 1g of tin iodide evenly, place them in a tubular muffle furnace, pass in argon as a protective gas, and raise the temperature of the furnace body at a heating rate of 1.5°C / min to 600°C, and keep the temperature constant for 3h. Then, the heating is stopped, and the furnace body is naturally lowered to room temperature, and the reaction product nitrogen-doped black phosphorus material is taken out.
[0048] (2) Preparation of nitrogen-doped phosphorene quantum dot materials:
[0049] Grind the nitrogen-doped black phosphorus material prepared in (1), and screen the powder with a particle size of 200 mesh, weigh 1g and place it in a 200mL beaker, add 100mL N-methylpyrrolidone as the dispersion medium, 0.1 g of europium trifluoromethanesulfonate was used as a stabilizer to obtain a mixed solution. The mixed solution was placed in an ultrasonic disperse...
Embodiment 3
[0053] (1) Preparation of nitrogen-doped black phosphorus material:
[0054] Blend 10g of red phosphorus, 2g of dicyandiamide, and 1g of tin iodide evenly, place them in a tubular muffle furnace, pass in argon as a protective gas, and increase the temperature of the furnace body at a heating rate of 1.5°C / min. Rise to 600 ° C, and keep the temperature for 3h. Then, the heating is stopped, and the furnace body is naturally lowered to room temperature, and the reaction product nitrogen-doped black phosphorus material is taken out.
[0055] (2) Preparation of nitrogen-doped phosphorene quantum dot materials:
[0056] Grind the nitrogen-doped black phosphorus material prepared in (1), and screen the powder with a particle size of 200 mesh, weigh 1g and place it in a 200mL beaker, add 100mL N-cyclohexylpyrrolidone in turn as the dispersion medium, 0.1 g of europium trifluoromethanesulfonate was used as a stabilizer to obtain a mixed solution. The mixed solution was placed in an ...
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