Ammonia gas adsorbent and preparation method thereof
An adsorbent and ammonia technology, applied in the field of environmental purification, can solve the problems of difficulty in forming porous materials, expansion, pulverization and agglomeration, and small contact area of ammonia, so as to increase the adsorption capacity, avoid pulverization and falling, The effect of increasing the contact area
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[0027] The present invention provides a method of preparing a ammonia adsorbent according to the above scheme, comprising the steps of:
[0028] Metal chloride is dissolved in a solvent to give a metal chloride solution;
[0029] Mix the molecular sieve with a metal chloride solution, dried to give an active component;
[0030] The active group was dispensed into a slurry coated on cordierite honeycomb ceramic to obtain ammonia absorbent.
[0031] The present invention dissolves the metal chloride in a solvent to obtain a metal chloride solution. In the present invention, the solvent is preferably water, methanol, ethanol. In the present invention, the concentration of the metal chloride solution is preferably 5% to 20%, more preferably 10% to 15% by weight, and more preferably 10% to 15% by weight.
[0032] After the metal chloride solution was obtained, the molecular sieve was mixed with a metal chloride solution to obtain an active component. In the present invention, the mixin...
Example Embodiment
[0036] Example 1
[0037] Active component preparation
[0038] The 20 g of ZSM-5 molecular sieves were mixed in a copper chloride solution having a concentration of 80 g of a mass concentration of 5%, and the molecular sieve was taken out in an oven at 80 ° C for 5 h at an oven at 80 ° C, then placed in chlorine after drying. Adsorption in the copper copper solution, repeat the above operation until the adsorption is completed, resulting in an active component.
[0039] 2. Application
[0040] The active component is uniformly dispersed in deionized water, and an aluminum sol binder (active component: binder: water mass ratio is 1: 1: 8), stirring at a rotational speed of 100 R / min for 2 h, then immersed in Bluestone honeycomb ceramics (active components are 30% of cordierite honeycomb ceramics), vacuum adsorption (vacuum is 0.5 MPa) 2min, take-out, purged, 100 ° C for 3 h, to obtain ammonia absorbent.
Example Embodiment
[0041] Example 2
[0042] Active component preparation
[0043] The 20 g of SAPO-34 molecular sieves were mixed in a calcium chloride solution having a concentration of 5 g of a concentration of 20%, and stirred at a rotational speed of 100 R / min for 2 h, and then dried in an oven at 70 ° C for 6 h to obtain an active component.
[0044] 2 coated
[0045] The active component is uniformly dispersed in deionized water, adding a silica sol binder (active component: binder: water mass ratio of 1: 0.5: 8.5), stirred at a speed of 100 r / min for 2 h, then immerse Bluestone honeycomb ceramics (active components are 25% of cordierite honeycomb ceramics), vacuum adsorption (vacuum is 0.1 MPa) 5 min, take it, purged, 110 ° C for 2.5 h, to obtain ammonia adsorbents.
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