Method for improving electronic glass reinforced size expansion phenomenon and preparation method of reinforced glass
A glass strengthening and electronic technology, which is applied in the preparation of strengthened glass and improves the size expansion of electronic glass strengthening. It can solve the problems of unusability, relaxation of tensile stress on the surface of glass products, and damage to product performance. It achieves short process and small expansion size. , Improve the effect of size expansion
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[0040] The preparation method of the potassium nitrate tempered salt comprises the following steps: preparing a mixed solution of ammonium nitrate and potassium chloride, crystallizing out the crude potassium nitrate, dissolving the crude potassium nitrate in water, adding potassium carbonate and potassium hydroxide, and stirring Filtrate, add nitric acid to the first filtrate, filter after stirring, add potassium hydroxide to the second filtrate to adjust the pH<7, crystallize and precipitate potassium nitrate tempered salt.
[0041] The preparation method of the sodium nitrate tempered salt comprises the following steps: preparing a mixed solution of ammonium nitrate and sodium chloride, crystallizing out the crude sodium nitrate, dissolving the crude sodium nitrate in water, adding sodium carbonate and sodium hydroxide, and stirring Filtrate, add nitric acid to the third filtrate, filter after stirring, add sodium hydroxide to the fourth filtrate to adjust the pH<7, crystall...
Embodiment 1
[0068] This embodiment provides a method for improving the size expansion phenomenon of electronic glass strengthening, the steps are as follows:
[0069] 1) Prepare potassium nitrate tempered salt with pH<7
[0070] Prepare a mixed solution of ammonium nitrate and potassium chloride according to ammonium ion: chloride ion = 1.5:1 (molar ratio), raise the temperature to 100°C, wait until the mixed solution evaporates to 40±2Be, and when potassium nitrate is saturated, it will be naturally crystallized Ensure that the temperature of the mixed solution drops to 35°C, and the crude potassium nitrate is precipitated. Dissolve the crude potassium nitrate in purified water, add potassium carbonate accounting for 0.5% of the total mass of the solution and potassium hydroxide accounting for 0.5% of the total mass of the solution, and stir for 2 hours. Finally, filter with 500 mesh filter gauze, add nitric acid accounting for 0.5% of the total mass of the solution in the filtered filtr...
Embodiment 2
[0083] This embodiment provides a method for improving the size expansion phenomenon of electronic glass strengthening, the steps are as follows:
[0084] 1) Prepare potassium nitrate tempered salt with pH<7
[0085] Prepare a mixed solution of ammonium nitrate and potassium chloride according to ammonium ion: chloride ion = 1.5:1 (molar ratio), raise the temperature to 100°C, wait until the mixed solution evaporates to 40±2Be, and when potassium nitrate is saturated, it will be naturally crystallized Ensure that the temperature of the mixed solution drops to 35°C, and the crude potassium nitrate is precipitated. Dissolve the crude potassium nitrate in purified water, add potassium carbonate accounting for 0.5% of the total mass of the solution and potassium hydroxide accounting for 0.5% of the total mass of the solution, and stir for 2 hours. Finally, filter with 500 mesh filter gauze, add nitric acid accounting for 0.5% of the total mass of the solution in the filtered filtr...
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