Glass PVB film with sound insulation and ultraviolet insulation functions and preparation method thereof
A glass and functional technology, applied in film/sheet release coatings, film/sheet adhesives, adhesives, etc., can solve the problem of glass PVB film sound insulation, poor UV blocking function, affecting the use efficiency of glass PVB film, etc. problem, to achieve the effect of enhancing sound insulation and anti-ultraviolet performance, enhancing sound insulation and anti-ultraviolet performance, and strong anti-pull performance
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Embodiment 1
[0020] S1: Mix and stir styrene-acrylic emulsion, polyurethane emulsion, and graphene according to the weight ratio of 3:2:1 to obtain a polymer emulsion;
[0021] S2: Send the shell powder into the maleic anhydride solution with a mass fraction of 30% according to the weight ratio of 1:3, then add the silane coupling agent KH550 with 10% shell powder, react at a temperature of 70°C for 20 minutes, and the reaction speed is 100r / min, the reaction is finished, and the grafted shell powder is obtained;
[0022] S3: Send lanthanum chloride into the phosphoric acid-hydrochloric acid buffer solution with a weight ratio of 3:1 for stirring treatment. The stirring temperature is 60°C, the stirring speed is 150r / min, and the stirring time is 20min. After the stirring is completed, then 100W laser Irradiation for 20min is processed to obtain modified lanthanum chloride for subsequent use;
[0023] Mix silicon dioxide and titanium dioxide at a weight ratio of 1:3, then add the modified...
Embodiment 2
[0029] S1: Mix and stir styrene-acrylic emulsion, polyurethane emulsion, and graphene according to the weight ratio of 3:2:1 to obtain a polymer emulsion;
[0030] S2: Send the shell powder into the maleic anhydride solution with a mass fraction of 40% according to the weight ratio of 1:3, then add the silane coupling agent KH550 with 10% shell powder, and react at a temperature of 90°C for 30 minutes, and the reaction speed is 500r / min, the reaction is finished, and the grafted shell powder is obtained;
[0031] S3: Lanthanum chloride is sent into the phosphoric acid-hydrochloric acid buffer solution obtained by the weight ratio of 3:1 for stirring treatment, the stirring temperature is 80°C, the stirring speed is 250r / min, the stirring time is 30min, the stirring is completed, and then the 500W laser Irradiated for 30 minutes to obtain modified lanthanum chloride;
[0032] Mix silicon dioxide and titanium dioxide according to a weight ratio of 1:3, then add the above-mentio...
Embodiment 3
[0040] S1: Mix and stir styrene-acrylic emulsion, polyurethane emulsion, and graphene according to the weight ratio of 3:2:1 to obtain a polymer emulsion;
[0041] S2: Send the shell powder into the maleic anhydride solution with a mass fraction of 35% according to the weight ratio of 1:3, then add the silane coupling agent KH550 with 10% shell powder, and react at a temperature of 80°C for 25 minutes, and the reaction speed is 300r / min, the reaction is finished, and the grafted shell powder is obtained;
[0042] S3: Send lanthanum chloride into the phosphoric acid-hydrochloric acid buffer solution with a weight ratio of 3:1 for stirring treatment. The stirring temperature is 70°C, the stirring speed is 200r / min, and the stirring time is 25min. After the stirring is completed, 300W laser radiation Treat according to 25min to obtain modified lanthanum chloride;
[0043] Mix silicon dioxide and titanium dioxide according to a weight ratio of 1:3, then add the above-mentioned mo...
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