A kind of photosensitive antibacterial and antioxidant composite fresh-keeping film based on nano bacterial cellulose and its preparation method and application
A nano-bacteria, composite preservation technology, applied in the chemical characteristics of fibers, chemical instruments and methods, single-component cellulose rayon, etc., can solve problems such as accidental ingestion, hidden dangers of food safety, and inability to remove, and reduce adverse effects. , the effect of reducing white pollution and alleviating environmental pressure
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Embodiment 1
[0047] The present embodiment provides a photosensitive composite fresh-keeping film based on nano-bacterial cellulose, and the preparation method thereof includes the following steps:
[0048] 1. Dispersion of Nanobacterial Cellulose Suspension
[0049] Deionized water was added to the purified bacterial cellulose with a mass percentage of 0.1%. At room temperature, the homogenization speed was 6000 r / min. After being treated with an ultra-high-speed homogenizer for 10 min, a certain amount of sodium lauryl sulfate was added. , treated with an ultrasonic cell disruptor for 5 min (frequency 15KHz), then added a certain amount of sodium lauryl sulfate, and ultrasonically treated for 5 min at room temperature until the bacterial cellulose was uniformly and stably dispersed in the water to obtain a nano-bacterial cellulose suspension. ,spare.
[0050] 2. Preparation of photodynamic antibacterial film
[0051] 20 parts of carboxymethyl chitosan solution with a degree of substitu...
Embodiment 2
[0059] The present embodiment provides a photosensitive composite fresh-keeping film based on nano-bacterial cellulose, and the preparation method thereof includes the following steps:
[0060] 1. Dispersion of Nanobacterial Cellulose Suspension
[0061] Deionized water was added to the purified bacterial cellulose with a mass percentage of 0.5%. At room temperature, the homogenization speed was 6000 r / min. After treatment with an ultra-high-speed homogenizer for 10 min, a certain amount of sodium lauryl sulfate was added. , treated with an ultrasonic cell disrupter for 5 min (frequency 15KHz), then added a certain amount of sodium dodecyl sulfate, and ultrasonically treated for 5 min at room temperature until the bacterial cellulose was uniformly and stably dispersed in the water to obtain a nano-bacterial cellulose suspension. ,spare.
[0062] 2. Preparation of photodynamic antibacterial film
[0063] 30 parts of carboxymethyl chitosan solution with a degree of substitutio...
Embodiment 3
[0071] The present embodiment provides a photosensitive composite fresh-keeping film based on nano-bacterial cellulose, and the preparation method thereof includes the following steps:
[0072] 1. Dispersion of Nanobacterial Cellulose Suspension
[0073] Deionized water was added to the purified bacterial cellulose with a mass percentage of 1%. At room temperature, the homogenization speed was 6000r / min. After being treated with an ultra-high-speed homogenizer for 10min, a certain amount of sodium lauryl sulfate was added. , treated with an ultrasonic cell disrupter for 5 min (frequency 15KHz), then added a certain amount of sodium dodecyl sulfate, and ultrasonically treated for 5 min at room temperature until the bacterial cellulose was uniformly and stably dispersed in the water to obtain a nano-bacterial cellulose suspension. ,spare.
[0074] 2. Preparation of photodynamic antibacterial film
[0075] Add 40 parts of carboxymethyl chitosan solution with a degree of substit...
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