Multi-stage high-specific-volume high-pressure aluminum foil formation method
A technology of high-voltage aluminum foil and formation method, which is applied in the manufacture of capacitors, electrolytic capacitors, and electrolytic capacitors. It can solve the problems of many formation steps, high boric acid content, and low conductivity, so as to reduce side reactions, improve CV performance, and product performance. Enhanced effect
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Embodiment 1
[0068] First, prepare the primary chemical forming liquid, secondary chemical forming liquid, tertiary chemical forming liquid and replenishing liquid according to the following process:
[0069] 1) Primary chemical conversion solution: add the main solute and auxiliary solute into deionized water, mix evenly, adjust the pH to 5 with ammonia water, and obtain the primary chemical conversion solution. The main solute is a mixture of ammonium adipate and ammonium suberate, the mass fraction of ammonium oxalate in the primary chemical solution is 5%, the mass fraction of ammonium suberate is 5%; the auxiliary solute is the mixture of citric acid and tartaric acid For the mixture, the mass fraction of citric acid in the primary conversion solution is 3%, and the mass fraction of tartaric acid is 2%.
[0070] 2) Secondary chemical formation solution: adding the main solute and auxiliary solute into deionized water, mixing evenly, and adjusting the pH to 5 with ammonia water to obta...
Embodiment 2
[0088] First, prepare the primary chemical forming liquid, secondary chemical forming liquid, tertiary chemical forming liquid and replenishing liquid according to the following process:
[0089] 1) Primary chemical conversion solution: add the main solute and auxiliary solute into deionized water, mix evenly, adjust the pH to 5 with ammonia water, and obtain the primary chemical conversion solution. The main solute is a mixture of ammonium adipate and ammonium suberate, the mass fraction of ammonium oxalate in the primary chemical solution is 4%, the mass fraction of ammonium suberate is 4%; the auxiliary solute is the mixture of citric acid and tartaric acid For the mixture, the mass fraction of citric acid in the primary conversion solution is 2%, and the mass fraction of tartaric acid is 2%.
[0090] 2) Secondary chemical formation solution: adding the main solute and auxiliary solute into deionized water, mixing evenly, and adjusting the pH to 5 with ammonia water to obta...
Embodiment 3
[0108] First, prepare the primary chemical forming liquid, secondary chemical forming liquid, tertiary chemical forming liquid and replenishing liquid according to the following process:
[0109] 1) Primary chemical conversion solution: add the main solute and auxiliary solute into deionized water, mix evenly, adjust the pH to 5 with ammonia water, and obtain the primary chemical conversion solution. The main solute is a mixture of ammonium adipate and ammonium azelate, the mass fraction of ammonium oxalate and ammonium azelate in the primary chemical solution is 3%; the auxiliary solute is citric acid and homophenylene For the mixture of triformic acid, the mass fraction of citric acid in the primary conversion solution is 1.5%, and the mass fraction of trimesic acid is 1.5%.
[0110] 2) Secondary chemical formation solution: adding the main solute and auxiliary solute into deionized water, mixing evenly, and adjusting the pH to 5 with ammonia water to obtain the secondary ch...
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