Preparation method of nanometer enhanced ultraviolet curing antifogging agent
A nano-enhanced, anti-fogging technology, applied in coatings, polyurea/polyurethane coatings, etc., can solve the problems of insufficient wear resistance, low hardness, limited application, etc., and achieve efficient dispersion, high hardness, and good water resistance. Effect
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[0027] The preparation method of the nano-enhanced ultraviolet curing antifogging agent of the present invention comprises the following steps:
[0028] (1) Preparation of carbon nitride nanoparticle dispersion
[0029] Under stirring conditions, add 1 mol / L sulfuric acid aqueous solution dropwise to 80°C, 0.5 mol / L melamine aqueous solution to form a white suspension, and continue stirring for 2 hours to obtain a precipitate; filter the precipitate and wash it with distilled water five times, Then washed three times with absolute ethanol, and dried at 60° C. for 24 hours to obtain melamine sulfate.
[0030] Mix and stir 3-5 parts by mass of melamine sulfate and 2-3 parts by mass of urea evenly, conduct heat treatment in a tube furnace, control the heating rate at 8°C / min, and heat-treat at 400°C for 8h; after naturally cooling to room temperature, Carbon nitride particles are obtained.
[0031] Mix 10 parts by mass of carbon nitride particles, 80 parts by mass of deionized ...
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