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Straw pulping method adopting complex enzyme preparation for pretreatment and application of straw pulping method in preparation of paper straws

A compound enzyme preparation and pretreatment technology, which is applied in the use of microorganisms/enzyme cellulose treatment, pulping with inorganic alkali, fiber raw material treatment, etc., can solve environmental pollution and other problems, reduce production costs, and avoid the use of chemical preparations , The effect of clear technical design thinking

Active Publication Date: 2022-03-15
QILU UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The traditional oxygen-alkali pulping process uses a large amount of alkali, accompanied by a large amount of organic waste liquid containing residual lignin and chemical substances, which has caused serious pollution to the environment

Method used

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  • Straw pulping method adopting complex enzyme preparation for pretreatment and application of straw pulping method in preparation of paper straws

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0051] A composite enzyme preparation includes: cellulase, xylan, laccase, lignin peroxidase, pectinase, and lipase, which is compounded in the form of an enzyme solution, and the composite enzyme preparation is in compound At the time of cellulase liquid, xyllase liquid, laccase, lignin peroxidase, pectin liquid and lipase solution of 10: 30: 20: 45: 25: 15, join Composite enzyme preparation 0.1% by weight of rat lump lipid; the cellulase liquid, xylosanil solution, lacquerade, lignin peroxidase, pectin liquid and lipase liquid 100,000 u / ml.

[0052] A straw pulping method preprocessed using a composite enzyme preparation, including the steps of:

[0053] 1) Squeeze and cleaning: Extrusion and cleaning straw, dry after drying, add water for 2 days;

[0054] 2) Enzyme preparation pretreatment: The infiltration straw is fed into the degradation tank, adding the above composite enzyme preparation according to 0.03% of the straw weight, mix uniform, mixing the enzyme of each enzyme...

Embodiment 2

[0060] A composite enzyme preparation includes: cellulase, xylan, laccase, lignin peroxidase, pectinase, and lipase, which is compounded in the form of an enzyme solution, and the composite enzyme preparation is in compound The volume ratio of the cellulase liquid, xylosaccharhase, laccase, ligno peroxidase, pectin liquid and lipase fluid is 13: 35: 25: 50: 30: 20, Composite enzyme preparation 0.1% by weight of rat lump lipid; the cellulase liquid, xylosanil solution, lacquerade, lignin peroxidase, pectin liquid and lipase liquid 100,000 u / ml.

[0061] A straw pulping method preprocessed using a composite enzyme preparation, including the steps of:

[0062] 1) Squeeze and cleaning: Extrusion and cleaning straw, dry after drying, add water for 2 days;

[0063] 2) Enzyme preparation pretreatment: The infiltration straw is fed into the degradation tank, adding the above composite enzyme preparation according to 0.1% of the straw weight, mix uniform, and the enzyme activity of each ...

Embodiment 3

[0069] A composite enzyme preparation includes: cellulase, xylan, laccase, lignin peroxidase, pectinase, and lipase, which is compounded in the form of an enzyme solution, and the composite enzyme preparation is in compound At the time of cellulase, xylosaccharse, laccase, lignin peroxidase, pectin solution and lipase solution of 15: 40: 30: 55: 35: 25, join Composite enzyme preparation 0.1% by weight of rat lump lipid; the cellulase liquid, xylosanil solution, lacquerade, lignin peroxidase, pectin liquid and lipase liquid 100,000 u / ml.

[0070] A straw pulping method preprocessed using a composite enzyme preparation, including the steps of:

[0071] 1) Squeeze and cleaning: Extrusion and cleaning straw, dry after drying, add water for 2 days;

[0072] 2) Enzyme preparation pretreatment: The infiltration straw is fed into the degradation tank, adding the above composite enzyme preparation according to 0.05% of the straw weight, mix well, adding the enzyme of each enzyme in the p...

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Abstract

The invention relates to a straw pulping method adopting complex enzyme preparation pretreatment and application of the straw pulping method in preparation of paper straws, and belongs to the technical field of pulping. The invention mainly provides a compound enzyme preparation for pretreating straws, the compound enzyme preparation is prepared by compounding cellulase liquid, xylanase liquid, laccase liquid, lignin peroxidase liquid, pectinase liquid and lipase liquid according to a volume ratio of (10-15): (30-41): (20-30): (45-55): (25-35): (15-25), and rhamnolipid accounting for 0.1-0.5 wt% of the compound enzyme preparation is added at the same time. All the enzymes have a synergistic effect, and efficient degradation of non-cellulose components in lignocellulose is jointly promoted. According to the method, pulping is extended, preparation of the paper straw by using the straw papermaking pulp is preliminarily explored, various indexes of the paper straw are preliminarily inspected, and the obtained paper straw is excellent in mechanical property.

Description

Technical field [0001] The present invention relates to a method of pulping straw pretreatment enzyme preparation and its application in making paper using the pipette, belonging to the technical field pulping. Background technique [0002] Paper industry is an important industrial material, but in recent years, domestic wood pulp phenomenon occurs shortage of raw materials, low-cost of straw pulp, straw-rich domestic resources urgently be exploited. [0003] Chinese Patent Document CN109734947A (Application No. 201910063921.5) discloses a straw Straw full biological degradation and its preparation method. Is obtained after pretreatment straw tube immersed in the cellulose solution, then taken out in air to form a gelled colloidal cellulose film tube surface straw, straw tube was placed in distilled water and then solvent exchange, dry naturally straw straw. Prepared in the above pipette technology, although biodegradable, but did not change the structure of the straw itself is t...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D21C5/00D21C3/02D21C3/22C12N9/24C12N9/02C12N9/08C12N9/20C12N9/18C12N9/42C12N9/88
CPCD21C5/005D21C3/02D21C3/222C12N9/2437C12N9/248C12N9/0061C12N9/0065C12N9/20C12N9/18C12N9/88C12N9/2402C12Y110/03002C12Y111/01014C12Y301/01003C12Y301/01011C12Y402/02002C12Y302/01015
Inventor 武玉康孙晗常德军刘泽同王腾飞黄迪
Owner QILU UNIV OF TECH