Fresh polygonatum odoratum freeze-dried decoction pieces and preparation method thereof
A Polygonatum Polygonatum and freeze-drying technology, which is applied in the field of traditional Chinese medicine, can solve problems such as cell damage and irritation, and achieve the effects of reducing calcium oxalate content, easy storage, and slowing down the rate of water sublimation
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Embodiment 1
[0026] A preparation method for freeze-dried decoction pieces of fresh Polygonatum odoratum comprises the following steps:
[0027] Step 1: After washing and removing impurities from the fresh Polygonatum odoratum, cut the thick slices into 0.6mm thick slices, put the thick slices into the acetic acid solution containing sesame oil for ultrasonic impregnation, take them out and dry them, and dry them in a nitrogen-filled oven with a drying wind speed of 8m / s; get the first crude product; the mass ratio of the sesame oil and the acetic acid solution is 1:1, and the concentration of the acetic acid solution is 10wt%;
[0028] Step 2: Put the first crude product into a fermentation broth containing oxalate decarboxylase for fermentation, ferment for 10 hours, and filter to obtain the second crude product;
[0029] Step 3: freeze-drying the second crude product under vacuum conditions to obtain the third crude product;
[0030] The preparation method of the fermented liquid is a...
Embodiment 2
[0033] A preparation method for freeze-dried decoction pieces of fresh Polygonatum odoratum comprises the following steps:
[0034] Step 1: After washing and removing impurities from the fresh Polygonatum odoratum, cut into 0.6mm thick slices, put the thick slices into acetic acid solution containing sesame oil for ultrasonic impregnation, take out and dry, and dry in a nitrogen-filled oven with a drying wind speed of 9m / s; get the first crude product; the mass ratio of the sesame oil and the acetic acid solution is 1:2, and the concentration of the acetic acid solution is 10wt%;
[0035] Step 2: putting the first crude product into a fermentation broth containing oxalate decarboxylase for fermentation, and obtaining the second crude product after the fermentation;
[0036] Step 3: freeze-drying the second crude product under vacuum conditions to obtain the third crude product;
[0037] The preparation method of the fermented liquid is as follows: dissolving oxalate decarbox...
Embodiment 3
[0040] A preparation method for freeze-dried decoction pieces of fresh Polygonatum odoratum comprises the following steps:
[0041] Step 1: After washing and removing impurities from the fresh Polygonatum odoratum, cut the thick slices into 0.8mm thick slices, put the thick slices into the acetic acid solution containing peanut oil for ultrasonic impregnation, take them out and dry them, and dry them in a nitrogen-filled oven with a drying wind speed of 9m / s; get the first crude product; the mass ratio of described peanut oil and acetic acid solution is 1:3, and the concentration of acetic acid solution is 12wt%;
[0042] Step 2: putting the first crude product into a fermentation broth containing oxalate decarboxylase for fermentation, and obtaining the second crude product after the fermentation;
[0043] Step 3: freeze-drying the second crude product under vacuum conditions to obtain the third crude product;
[0044] The preparation method of the fermented liquid is as fo...
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