Preparation method and application of carbon nanoparticles
A technology of carbon nano-particles, dehydration and carbonization, applied in nano-carbon, nano-technology, nano-optics, etc., to achieve the effects of low process cost, high-efficiency light-to-heat conversion characteristics, and simple preparation methods
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0035] The preparation of embodiment 1 carbon nanoparticle
[0036] Dissolve 1g of citric acid and 2g of ammonium carbonate in 30mL of DMSO solvent to obtain a transparent solution, then place it in a 50mL polytetrafluoroethylene autoclave, react at 160°C for 4 hours, the reaction pressure is 7MPa, and the solution after the reaction is filtered Finally, a powdery solid is obtained, and the powdery solid is washed with water, centrifuged (8000rpm, 5min), dried and other processes to obtain a dark blue powder, that is, to obtain carbon nanoparticles.
[0037] Observe the shape and size of carbon nanoparticles by TEM (transmission electron microscope) and AFM (atomic force microscope), such as Figure 1-Figure 3 As shown, it shows that the size of carbon nanoparticles synthesized in this example is about 2-15nm, and the height is about 1-15nm.
[0038] Observe the elements on the surface of carbon nanoparticles and the composition of surface functional groups by EDS (X-ray ener...
Embodiment 2
[0039] The preparation of embodiment 2 carbon nanoparticles
[0040] Dissolve 1g of ethylenediaminetetraacetic acid and 10g of ammonium acetate in 10mL of DMF solvent to obtain a transparent solution, then place it in a 50mL polytetrafluoroethylene autoclave, react at 220°C for 1 hour, and the reaction pressure is 2MPa. After the solution is filtered, a powdery solid is obtained, and the powdery solid is washed with water, centrifuged (8000rpm, 5min), dried and other processes to obtain a dark blue powder, that is, carbon nanoparticles.
[0041] The morphology and size of the carbon nanoparticles were observed by TEM and AFM, and the result was similar to that of Example 1, and the size of the synthesized carbon nanoparticles was about 2-15nm.
[0042] The elements on the surface of carbon nanoparticles and the composition of surface functional groups were observed by EDS and FTIR. The result was similar to that of Example 1. The surface of the synthesized carbon nanoparticles...
Embodiment 3
[0043] The preparation of embodiment 3 carbon nanoparticles
[0044] Dissolve 2g of glucose and 1g of ammonium chloride in 50mL of THF solvent to obtain a transparent solution, then place it in a 50mL polytetrafluoroethylene autoclave, react at 110°C for 12 hours, and the reaction pressure is 10Mpa, and the reacted solution is filtered Finally, a powdery solid is obtained, and the powdery solid is washed with water, centrifuged (8000rpm, 5min), dried and other processes to obtain a dark blue powder, that is, to obtain carbon nanoparticles.
[0045] The morphology and size of the carbon nanoparticles were observed by TEM and AFM, and the result was similar to that of Example 1, and the size of the synthesized carbon nanoparticles was about 2-15nm.
[0046] Observe the elements on the surface of carbon nanoparticles and the composition of surface functional groups by EDS and FTIR. The result is similar to Example 1. The surface of the synthesized carbon nanoparticles is rich in a ...
PUM
| Property | Measurement | Unit |
|---|---|---|
| size | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More