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High-temperature and high-pressure silicon carbide printed circuit board heat exchanger and preparation method thereof

A printed circuit board, high temperature and high pressure technology, applied in the direction of indirect heat exchangers, heat exchanger types, heat exchange equipment, etc., can solve the problems of difficult industrial scale-up, no general design standards, and no wide application

Pending Publication Date: 2022-07-08
QINGDAO UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, due to the low pressure of silicon carbide, the lack of current general design standards, and the difficulty of industrial scale-up, it has not been widely used.

Method used

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  • High-temperature and high-pressure silicon carbide printed circuit board heat exchanger and preparation method thereof
  • High-temperature and high-pressure silicon carbide printed circuit board heat exchanger and preparation method thereof
  • High-temperature and high-pressure silicon carbide printed circuit board heat exchanger and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment example 1

[0030] The carbon powder and silicon powder are made into mixed powder according to the molar ratio of 1:1, and the grinding ball and the grinding powder are packaged in an argon gas tank according to the mass ratio of 30:1, and the mechanical ball milling is carried out on a ball mill, and the average grain size is obtained after 1 day. 50nm silicon carbide powder.

[0031] Add the alcoholic solution of o-methylcellulose or polyvinyl alcohol as a binder, and then form a blank in a steel film with a pressure of 70MPa. Sintered under argon for 3 hours.

[0032] Using the diamond sawing method, the holes and microchannels of each component were carved on the silicon carbide billet, and then placed in a high-temperature sintering furnace again, the temperature was kept at 1900 ° C, and sintered for 2 hours under flowing argon gas of 1 atm.

[0033] Take out the sintered silicon carbide, grind it flat, and wet-process the ground silicon carbide. Then, the ion system is used to a...

Embodiment example 2

[0036] The carbon powder and silicon powder are made into mixed powder according to the molar ratio of 1:1, and the grinding ball and the grinding powder are packaged in an argon gas tank according to the mass ratio of 30:1, and the mechanical ball milling is carried out on a ball mill, and the average grain size is obtained after 1 day. 100nm silicon carbide powder.

[0037] Add the alcoholic solution of o-methylcellulose or polyvinyl alcohol as a binder, and then form a blank in a steel film with a pressure of 100MPa. Sintered under argon for 3 hours.

[0038] Using the diamond sawing method, the holes and microchannels of each component are carved on the silicon carbide blank, and then placed in a high-temperature sintering furnace again, the temperature is kept at 2200 ° C, and sintered for 2 hours under flowing argon gas of 1 atm.

[0039] Take out the sintered silicon carbide, grind it flat, and wet-process the ground silicon carbide. Then the ion system is used to act...

Embodiment example 3

[0042] The carbon powder and silicon powder are made into mixed powder according to the molar ratio of 1:1, and the grinding ball and the grinding powder are packaged in an argon gas tank according to the mass ratio of 30:1, and the mechanical ball milling is carried out on a ball mill, and the average grain size is obtained after 1 day. 200nm silicon carbide powder.

[0043]Add the alcoholic solution of o-methylcellulose or polyvinyl alcohol as a binder, and then form a blank in a steel film with a pressure of 200MPa. Sinter under flowing argon for 3 hours.

[0044] Using the diamond sawing method, the holes and microchannels of each component are carved on the silicon carbide blank, and then placed in a high-temperature sintering furnace again, the temperature is kept at 2200 ° C, and sintered for 2 hours under flowing argon gas of 1 atm.

[0045] Take out the sintered silicon carbide, grind it flat, and wet-process the ground silicon carbide. Then, the ion system is used ...

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Abstract

The invention discloses a high-temperature and high-pressure silicon carbide printed circuit board heat exchanger and a preparation method thereof. The high-temperature and high-pressure silicon carbide printed circuit board heat exchanger comprises a cold fluid printed circuit board, a hot fluid printed circuit board, an upper baffle, a lower baffle, a cold fluid outlet integrated flange, a hot fluid outlet integrated flange, a cold fluid inlet integrated flange, a hot fluid inlet integrated flange and a graphite self-sealing connecting structure. The preparation method comprises the following steps: preparing carbon powder and silicon powder into mixed powder according to a molar ratio of 1: 1, packaging the mixed powder and grinding balls in an argon tank, carrying out mechanical ball milling on a ball mill for 1 day to obtain silicon carbide nano-powder, adding a binding agent, carrying out high-pressure blank forming in a steel film, carving, and carrying out pressureless sintering to obtain the silicon carbide nano-powder. And after sintering, taking out and polishing again, and bonding the whole body. The preparation method has the advantages that the prepared silicon carbide printed circuit board heat exchanger solves the problem that a metal printed circuit board heat exchanger is not resistant to corrosion; the silicon carbide printed circuit board heat exchanger can bear high pressure of 30 MPa through the machining technology, the connection structure is improved so that the connection position of the silicon carbide printed circuit board heat exchanger can bear the high temperature of 600 DEG C and the high pressure of 30 MPa at the maximum at the same time, and the industrial amplification requirement of the silicon carbide printed circuit board heat exchanger is met.

Description

technical field [0001] The invention relates to a high temperature and high pressure printed circuit board heat exchanger and a preparation method thereof, in particular to a high temperature and high pressure silicon carbide printed circuit board heat exchanger and a preparation method thereof. Background technique [0002] With the gradual reduction of fossil fuels and the serious environmental pollution caused by their combustion, renewable green energy such as solar energy and nuclear energy has attracted much attention. [0003] Among them, supercritical CO 2 (S-CO 2 ) energy storage power generation technology, as a cutting-edge technology that has developed rapidly in recent years, has been widely studied by scholars at home and abroad. Compared with the traditional steam Rankine cycle power generation system, under the same turbine inlet working fluid temperature, S-CO 2 The energy storage power generation system has higher cycle efficiency; adopts S-CO 2 As a cl...

Claims

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Application Information

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IPC IPC(8): F28D9/00F28F3/08F28F21/00
CPCF28D9/0037F28F3/086F28F21/00F28F2260/02Y02P20/10
Inventor 胡德栋韩俊杰段淑娜于国栋李瑶徐琦柒远贞
Owner QINGDAO UNIV OF SCI & TECH