Catalytic pyrolysis method for preparing LGO
A catalytic pyrolysis and catalyst technology, applied in chemical instruments and methods, preparation of sugar derivatives, physical/chemical process catalysts, etc., can solve the problems of acid site loss, catalysts that cannot be recovered and regenerated, and difficult to exist stably, so as to promote Depolymerization, achieve high yield and high selectivity preparation, good adsorption effect
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0026] Weigh 54g NbCl 5 The mixed gel was prepared with 10g CTAB, placed in a hydrothermal kettle for aging at 160°C for 24h, then washed with deionized water to pH=7, then dried in an oven at 80°C for 12h, and finally calcined at 450°C 6h to obtain mesoporous niobium oxide.
[0027] Take 10g of the mesoporous niobium oxide prepared above, and another 6.1g of NH 4 H 2 PO 4 Dissolved in a certain amount of deionized water to make a solution, and the NH 4 H 2 PO 4 Loaded on mesoporous niobium oxide, ultrasonicated for 30 min, then dried in an oven at 80 °C for 12 h, taken out and calcined at 450 °C for 4 h to obtain NH 4 H 2 PO 4 Modified mesoporous niobium oxide, in which phosphate accounts for 50% by mass.
[0028] Take 10 g of NH prepared above 4 H 2 PO 4 The modified mesoporous niobium oxide was ground to 0.2 mm, and commercial microcrystalline cellulose was used as the raw material (average particle size was 0.05 mm), and the cellulose and the catalyst were mixe...
Embodiment 2
[0030] Weigh 107g C 10 H 5 NbO 20 The mixed gel was prepared with 10g CTAB, placed in a hydrothermal kettle for aging at 150°C for 24h, then washed with deionized water to pH=7, then dried in an oven at 80°C for 12h, and finally calcined at 450°C 6h to obtain mesoporous niobium oxide.
[0031]Take 10g of the mesoporous niobium oxide prepared above, and another 5.5g (NH 4 ) 2 HPO 4 It was dissolved in a certain amount of deionized water to make a solution, and the (NH) 4 ) 2 HPO 4 Loaded on mesoporous niobium oxide, ultrasonicated for 30 min, then placed in an oven to dry at 80 °C for 12 h, taken out and calcined at 450 °C for 5 h to obtain (NH 4 ) 2 HPO 4 Modified mesoporous niobium oxide, in which phosphate accounts for 40% by mass.
[0032] Take 10 g of (NH) prepared above 4 ) 2 HPO 4 The modified mesoporous niobium oxide was ground to 0.2 mm, and commercial microcrystalline cellulose was used as the raw material (average particle size was 0.05 mm), and the cel...
Embodiment 3
[0034] Weigh 64g C 4 H 4 NNbO 9 ·nH 2 O and 10g CTAB were prepared as mixed gel, which was aged in a hydrothermal kettle at 180°C for 24h, then washed with deionized water to pH=7, then dried in an oven at 80°C for 12h, and finally at 450°C After calcination for 6h, mesoporous niobium oxide was obtained.
[0035] Take 10g of the mesoporous niobium oxide prepared above, and another 9.3g (NH 4 ) 3 PO 4 It was dissolved in a certain amount of deionized water to make a solution, and the (NH) 4 ) 3 PO 4 Loaded on mesoporous niobium oxide, ultrasonicated for 30 min, then placed in an oven to dry at 80 °C for 12 h, taken out and calcined at 450 °C for 3 h to obtain (NH4) 3 PO 4 Modified mesoporous niobium oxide, in which phosphate accounts for 60% by mass.
[0036] Take 10 g of (NH) prepared above 4 ) 3 PO 4 The modified mesoporous niobium oxide was ground to 0.2 mm, and commercial microcrystalline cellulose was used as the raw material (average particle size was 0.05 m...
PUM
Login to view more Abstract
Description
Claims
Application Information
Login to view more - R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap