Method for preparing electromagnetic shielding compound material
A technology of electromagnetic shielding materials and composite materials, applied in the direction of magnetic field/electric field shielding, electrical components, etc., can solve the problem of high cost, achieve the effect of light weight, low density, and prevent malfunction
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Embodiment 1
[0018] The dry woody material-straw husk was selected as the raw material, treated at 250°C for 1 hour at a heating rate of 1°C / min under non-oxygen conditions, and then immersed in the aqueous solution of magnetic metal salt-nickel carbonate for 1 hour, then taken out and dried. The treated and dried rice straw husk powder is fully mixed with the modified resin-phenolic resin, and then press-molded at 100°C and 10MPA pressure, and further heated to 250°C at a rate of 1°C / min under a non-oxygen inert atmosphere. Incubate for 1 hour for non-oxidative treatment. Spray ABS resin on the sample after high temperature treatment, with a thickness of 50um, and prepare an electromagnetic shielding composite material with a shielding effect of more than 50dB in the range of 150MHZ-1.5GHZ after curing at room temperature.
Embodiment 2
[0020] Select dry woody material-rice bran as raw material, treat it at 650°C for 8 hours at a heating rate of 20°C / min under non-oxygen conditions, then immerse it in the aqueous solution of magnetic metal salt-ferric chloride for 24 hours, then take it out and dry it. Fully mix the treated and dried bran material powder with the modified resin-furan resin, press it at 350°C and 50MPA pressure, and further raise the temperature to 1500°C at a rate of 20°C / min in a non-oxygen inert atmosphere , Insulated for 6 hours for non-oxidative treatment. Spray acrylic resin on the sample after high temperature treatment with a thickness of 1000um, and prepare an electromagnetic shielding composite material with a shielding effect of more than 65dB in the range of 150MHZ-1.5GHZ after curing at room temperature.
Embodiment 3
[0022] Select the dry woody material-sorghum shell as the raw material, treat it at 450°C for 3 hours at a heating rate of 1°C / min under non-oxygen conditions, and then immerse it in the aqueous solution of magnetic metal salt-nickel nitrate for 12 hours, then take it out and dry it. Fully mix the treated and dried sorghum shell material powder with the modified resin-furfural resin, press it at 250°C and 30MPA pressure, and further raise the temperature to 875°C at a rate of 10°C / min in a non-oxygen inert atmosphere , heat preservation for 4 hours for non-oxidative treatment. Spray organic silicone resin on the sample after high temperature treatment with a thickness of 500um, and prepare an electromagnetic shielding composite material with a shielding effect of more than 60dB in the range of 150MHZ-1.5GHZ after curing at room temperature.
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