Preparation method of metal sulfide semiconductor nanocrystalline
A technology of metal sulfides and semiconductors, applied in semiconductor/solid-state device manufacturing, sulfur compounds, nanostructure manufacturing, etc., can solve the problems of metal sulfide semiconductor nanomaterials that have not yet been seen, and achieve easy construction, good crystallinity, and purity high effect
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0016] The first step is to immerse the flat and smooth glass sheet in the commercially available collodion solution (C.R. grade, Shanghai bronzing material factory), repeat the pulling twice, and dry it naturally. The thickness on the glass sheet is about 0.2mm. Uniform, artificial active membrane whose size can be made according to the shape and size of the reactor.
[0017] In the second step, take 0.1mol / L of Hg(NO 3 ) 2 Solution 20mL and 0.1mol / L Na 2 20 mL of S solution was placed on both sides of the artificial active membrane, stirred with a 6511 electric mixer from Shanghai Standard Mold Factory, and reacted at room temperature for 48 hours. The reaction solution on both sides of the artificial active membrane was taken out, subjected to conventional centrifugation, and discarded for clarification. liquid, leaving the product. Next, wash with commercially available chemically pure acetone and deionized water in sequence. Remove the artificial active membrane, wash...
Embodiment 2
[0019] With 0.10mol / L CdCl 2 Solution 20mL replaces 0.10mol / L of Hg(NO 3 ) 2 Solution, other conditions and steps are exactly the same as in Example 1, and the obtained product is a spherical cadmium sulfide quasi-nanocrystal, and the average particle size of the product is 170nm. The performance is basically the same as that of HgS nanocrystals.
Embodiment 3
[0021] The first step is the same as in Example 1 except that the thickness of the artificial active film is 0.4 mm. In the second step, take 0.15mol / L AgNO 3 Solution 40ml and 0.15mol / L Na 2 20ml of S solution was placed on both sides of the artificial active membrane. The whole system was placed in a dark place. The active membrane was washed sequentially with acetone and deionized water and combined to obtain Ag 2 S nanocrystal, after testing, the optical performance is the same as before, and the average particle size of the product is 28nm.
PUM
Property | Measurement | Unit |
---|---|---|
thickness | aaaaa | aaaaa |
particle size | aaaaa | aaaaa |
particle size | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com