Method of coating abrasives
A coating, thermal coating technique applied to tantalum or, abrasive grit, carbide precursors to achieve high temperature effects
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Embodiment 1
[0038] Diamond grit from ElementSix, 40 / 45 US mesh size, was CVD coated according to general methods generally known in the art, resulting in TiC-coated diamonds. CVD TiC-coated diamond was then used as the substrate for the second coating step.
[0039] 3000 carats of this TiC-coated diamond, 40 / 45 US mesh size, were placed into a magnetron sputter coater with a rotating cylinder and a large plate of pure titanium metal as the target. The coating chamber is evacuated, argon gas is admitted, and the power is turned on to form a plasma. The sputtering power was increased to 5000W while rotating the cylinder to ensure a uniform coating on all diamond particles. Two 160 minute sputtered titanium runs were continued with samples taken after the first run for analysis before continuing. The coated diamond is allowed to cool before being removed from the chamber.
[0040] After the second test, an analysis of the coated diamond was carried out by means of X-ray diffraction, X-ray...
Embodiment 2
[0043] CVD TiC-coated diamonds were produced as in Example 1. This TiC-coated diamond was then used as the substrate for the second coating step. 500 carats of this TiC-coated diamond, 40 / 45 US mesh size, were placed into a magnetron sputter coater with a rotating cylinder and a large plate of pure titanium metal as the target. The coating chamber is evacuated, argon gas is admitted, and the power is turned on to form a plasma. The sputtering power was increased to 5000W while rotating the cylinder to ensure a uniform coating on all diamond particles. Continue to sputter titanium metal for 120 minutes. The coated diamond is allowed to cool before being removed from the chamber.
[0044] The analysis of the coated diamond was carried out, consisting of X-ray diffraction, X-ray fluorescence, chemical determination of the coating, optical and scanning electron microscopy image analysis and particle breakage followed by cross-sectional analysis on the SEM .
[0045] To the na...
Embodiment 3
[0047] CVD TiC-coated diamonds were produced as in Example 1. This TiC-coated diamond was then used as a substrate for the coating. 1000 carats of this TiC-coated diamond, 40 / 45 US mesh size, were placed into a magnetron sputter coater with a rotating cylinder and a large plate of pure silicon metal as the target. The coating chamber is evacuated, argon gas is admitted, and the power is turned on to form a plasma. The sputtering power was increased to 5A (400V) on the target while rotating the cylinder to ensure a uniform coating on all diamond particles at 20 sccm argon pressure. Butane gas was admitted to achieve a pressure of 30 seem. The sputtering of silicon reacted with carbon was continued for 5 hours. The coated diamond is allowed to cool before being removed from the chamber.
[0048] The analysis of the coated diamond was carried out, consisting of X-ray diffraction, X-ray fluorescence, chemical determination of the coating, optical and scanning electron microsco...
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Abstract
Description
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