Film-Forming Composition, Film Formed Thereby, and Method for Manufacturing Organic Semiconductor Element Using Same
a film-forming composition and film-forming technology, applied in the field of film-forming composition and film-forming process, can solve the problem of difficulty in obtaining film-forming compositions that satisfy both requirements
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synthesis example 1
Comparative Resin Synthesis Example 1
[0203]In a reaction vessel, 5.00 g (35.2 mmol) of n-butyl methacrylate, 10.0 g of butanone and 0.162 g (0.704 mmol) of initiator were placed. The resulting solution was subjected to radical polymerization by the method described in the above section “Synthesis of Fluororesins”. As a result, there was obtained 0.88 g of fluororesin 14 having a repeating unit of the following formula (22). The weight-average molecular weight Mw of the fluororesin 14 was 16,000. The molecular weight distribution Mw / Mn of the fluororesin 14 was 1.48. The yield of the fluororesin 14 relative to the total mass of the monomer used was 18 mass %.
synthesis example 2
Comparative Resin Synthesis Example 2
[0204]In a reaction vessel, 10.00 g (63.2 mmol) of 2-ethoxyethyl methacrylate, 10.0 g of butanone and 0.225 g (0.977 mmol) of initiator were placed. The resulting solution was subjected to radical polymerization by the method described in the above section “Synthesis of Fluororesins”. As a result, there was obtained 6.21 g of fluororesin 15 having a repeating unit of the following formula (23). The weight-average molecular weight Mw of the fluororesin 15 was 8,000. The molecular weight distribution Mw / Mn of the fluororesin 15 was 1.45. The yield of the fluororesin 15 relative to the total mass of the monomer used was 62 mass %.
[0205][Evaluation Test on Solubility of Fluororesins in Fluorine-Containing Solvents]
[0206]The fluororesins 1 to 13, the comparative fluorine-free resins 14 and 15 and polymethyl methacrylate (hereinafter sometimes referred to as “PMMA”; polystyrene-conversion weight-average molecular weight: 15,000) available from Sigma-Al...
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