The invention discloses a preparation method of temperature-adjusting
Lyocell fibers loaded with
phase change microcapsules, and belongs to the technical field of
phase change materials. The method comprises the following steps: 1) reacting SMA with a
sodium hydroxide solution, and adjusting the pH value with a
citric acid solution to obtain an emulsifier, wherein the SMA accounts for 4-6% of the total
mass of the emulsifier; carrying out high-speed shearing emulsification on an emulsifier and n-
octadecane for 20-40 minutes to form an oil-in-water
emulsion, dropwise adding the melamino-
formaldehyde prepolymer under mechanical stirring, and reacting to obtain a
phase change microcapsule; and 2) uniformly dispersing the phase change microcapsules into 45-55wt% of an NMMO
aqueous solution, then removing water to increase the concentration of the NMMO to 80-90%, then sequentially adding
propyl gallate and wood pulp
powder, and after the wood pulp
powder is completely dissolved, carrying out wet
spinning to obtain the phase change microcapsule loaded temperature-regulating
Lyocell fiber. The obtained
fiber is small in
diameter, has high
enthalpy heat and good temperature adjusting capability, and is wide in application prospect.