Method for preventing hydrophobic chemical protection layer on immovable cultural artifact surface desquamating
A protective layer, hydrophobic technology, applied in the direction of the device, coating, building structure, etc. to apply liquid on the surface, to achieve the effect of good permeability and weather resistance, and alleviate the damage
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Embodiment 1
[0021] A hydroxyacrylic microemulsion was first prepared. After hydroxyethyl methacrylate, methyl methacrylate, butyl acrylate and acrylic acid were removed from the polymerization inhibitor, they were formulated into a monomer mixture in a ratio of 3.5:5.0:6.3:0.2; Add the calculated amount of the aqueous solution of the emulsifier sodium lauryl sulfate and the co-emulsifier cyclohexane dissolved by the ultrasonic cleaner to the four-necked flask with the thermometer, the condenser tube and the dropping funnel, and then add 1 / 4 of the prepared The monomer mixed solution; the temperature of the water bath was raised to 75°C, and after 30 minutes of nitrogen gas, half of the initiator ammonium persulfate accounting for 0.05 of the total monomer mass was added, and then the remaining 3 / 4 of the monomer mixed solution was added dropwise within 2 hours. The remaining 1 / 2 of the initiator; followed by heat preservation reaction for 1 hour; cooling to 40°C, adding ammonia water drop...
Embodiment 2
[0031] Same as Example 1, except that the fluororubber solution is changed into a silicone solution, that is, 8% partially polymerized cetyltrimethoxysilane butyl acetate solution is used as the surface layer chemical protection agent. Results The sandstone sample protected by three layers of chemical protection went through 7 damage cycle experiments, and it was found that there was a slight damage between the protected part and the unprotected part on the side surface of the sample, with a mass loss rate of 4.2%, and a water contact angle of the protected surface from 119 degrees is reduced to 93 degrees, and the antifouling effect on blue ink is reduced (from 5 points to 3 points). The reversible rate of one suction is about 14%.
[0032] The control experiment of embodiment 2
[0033] Same as Example 2, except that the chemical protective agent of the base layer and the chemical protective agent of the transition layer are impermeable, that is, the surface monolayer is pr...
Embodiment 3
[0035] Same as Example 1, except that the chemical protection of the transition layer is not implemented, that is, only the hydroxyacrylic acid microemulsion and the fluorine rubber solution are used for double-layer chemical protection. Results After 7 cycles of failure experiments on the sandstone sample, the surface of the sample did not show any change, the mass loss rate of the sample increased slightly to 1.2%, and the contact angle of the protected surface decreased from 113 degrees to 91 degrees. The antifouling effect is basically unchanged, that is, 5 points remain unchanged. The reversible rate of one suction is about 21%.
[0036] The control experiment of embodiment 3
[0037] Same as Example 3, except that the fluororubber solution is changed into a silicone solution, that is, 8% partially polymerized cetyltrimethoxysilane butyl acetate solution is used as the surface layer chemical protection agent. Results After 7 times of damage cycle experiments on the sand...
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