Rotary pouring manufacture method of AZ91D magnesium alloy semisolid slurry

A technology of semi-solid slurry and rotary casting, which is applied in the field of metal material forming, and can solve the problems of short life of mixing chamber and stirring rod, easy pollution of semi-solid alloy slurry, low production efficiency of mechanical stirring method, etc., and achieves compact structure, Fine grain structure and strong practical effect

Inactive Publication Date: 2009-02-11
NANCHANG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Each method has its own disadvantages. The traditional mechanical stirring method has low production efficiency, short service life of the stirring chamber and stirring rod, and the stirring rod and stirring chamber are easy to pollute the semi-solid alloy slurry, which is only suitable for laboratory research work. , cannot meet the needs of commercial production; due to the existence of "skin effect", the electromagnetic stirring method is generally considered to be only able to prepare semi-solid slurry with a diameter of less than 150mm, and the energy consumption is large; the attenuation of ultrasonic vibration waves in the ultrasonic vibration method is severe, Ultrasonic waves cannot reach deeper or farther areas; the deformation mutagenesis activation method requires a large amount of extrusion deformation, so only small-diameter alloy semi-solid billets can be prepared; semi-solid billets prepared by spray deposition are expensive and only suitable for It is suitable for preparing advanced or refractory alloy blanks and forming advanced part blanks, and it cannot be applied on a large scale

Method used

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  • Rotary pouring manufacture method of AZ91D magnesium alloy semisolid slurry
  • Rotary pouring manufacture method of AZ91D magnesium alloy semisolid slurry
  • Rotary pouring manufacture method of AZ91D magnesium alloy semisolid slurry

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] The invention is a slurry preparation process of AZ91D magnesium alloy, the chemical composition (mass fraction, %) of the alloy is: Al-8.920, Zn-0.617, Mn-0.208, Si-0.023, Fe-0.002, Cu-0.001, Be -0.001, Ni-0.001, the rest is Mg. The alloy has a liquidus temperature of 595°C and a solidus temperature of 470°C. The specific process is as follows:

[0022] (1) Melt the AZ91D magnesium alloy at a high temperature of 710°C in a melting furnace and refine it for 1 hour; then cool the AZ91D magnesium alloy melt to a pouring temperature of 630°C and keep it warm for 15 minutes to make the temperature and chemical composition of the AZ91D magnesium alloy melt uniform change.

[0023] (2) Rotary pouring: first, the preheating temperature of the rotary pouring tube is 60°C, the rotational speed of the rotary pouring tube is 0r / min, and the inclination angle of the rotary pouring tube is 25 degrees, and the above-mentioned AZ91D magnesium alloy melt is poured into the rotary cas...

Embodiment 2

[0026] The magnesium alloy described in Example 1.

[0027] (1) Melt the AZ91D magnesium alloy at a high temperature of 710°C in a melting furnace and refine it for 1 hour; then cool the AZ91D magnesium alloy melt to a pouring temperature of 630°C and keep it warm for 15 minutes to make the temperature and chemical composition of the AZ91D magnesium alloy melt uniform change.

[0028] (2) Rotary casting: first, the preheating temperature of the rotary casting tube is 60°C, the rotating speed of the rotary casting tube is 75r / min, and the inclination angle of the rotary casting tube is 30 degrees, and the above-mentioned AZ91D magnesium alloy melt is poured into the rotary casting tube through the guide tube .

[0029] (3) The crystallizer was preheated to a temperature of 475°C, and the AZ91D magnesium alloy melt flowed into the crystallization furnace, and kept for 8 minutes.

Embodiment 3

[0031] The magnesium alloy described in Example 1.

[0032] (1) Melt the AZ91D magnesium alloy at a high temperature of 710°C in a melting furnace and refine it for 1 hour; then cool the AZ91D magnesium alloy melt to a pouring temperature of 635°C and keep it warm for 15 minutes to make the temperature and chemical composition of the AZ91D magnesium alloy melt uniform change.

[0033] (2) Rotary pouring: first, the preheating temperature of the rotary pouring tube is 60°C, the rotational speed of the rotary pouring tube is 45r / min, and the inclination angle of the rotary pouring tube is 20 degrees, and the above alloy melt is poured into the rotary pouring tube through the guide tube.

[0034] (3) The crystallizer was preheated to a temperature of 480°C, and the AZ91D magnesium alloy melt flowed into the crystallization furnace, and kept warm for 6 minutes. Example 4.

[0035] The magnesium alloy described in Example 1.

[0036] (1) Melt the AZ91D magnesium alloy at a high ...

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Abstract

The invention relates to a method for preparing AZ91D magnesium alloy semi-solid sizing agent by rotating pouring, which is characterized in that AZ91D magnesium alloy is melted and refined in a smelting maintaining furnace, then cooled to 630-650 DEG C, and insulated for 10-30 minutes; a stainless steel rotating pouring tube is preheated to 60-80 DEG C, with the rotating speed of the pouring tube controlled at 0-105r / min, and the inclination of the rotating pouring tube being 20-30 degrees; then the AZ91D magnesium alloy melt is poured into the rotating tube through a deflection tube; a crystallizer is preheated to 470-500 DEG C; the AZ91D magnesium alloy melt enters the crystallizer through the rotating pouring tube, and insulated for 5-15 minutes. The method for preparing the AZ91D magnesium alloy semi-solid sizing agent by rotating pouring has a simple device, low cost, convenient operation, high practicality; the prepared AZ91D magnesium alloy semi-solid sizing agent has fine grain organization and even distribution; in addition, the process flow is short, the energy consumption is low, the efficiency is high, the equipment is simple, the structure is compact, the applicability is high, and the method is especially applicable to small and medium-sized enterprises of China.

Description

technical field [0001] The invention belongs to the technical field of metal material forming, and relates to a preparation method of magnesium alloy semi-solid slurry. Background technique [0002] As a light metal, magnesium alloy is second only to titanium alloy and alloy structural steel in terms of specific strength and specific stiffness. It is not only much higher than engineering materials, but also significantly higher than aluminum alloy. Its impact resistance, processing performance and recyclability are all better than aluminum alloy. alloy. Because of these excellent properties of magnesium, magnesium and its alloys have been widely used in aviation, aerospace, navigation, communication, transportation, audio and video equipment, microelectronics technology and other fields in recent years. Magnesium alloys have excellent thin-wall casting performance, good specific strength, specific stiffness and anti-collision ability, which can fully meet the requirements o...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B22D21/04
Inventor 杨湘杰郭洪民叶寒王明王小康万正东程尚栩
Owner NANCHANG UNIV
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