Ceramic-base compound material and forming technique
A technology of composite materials and forming technology, which is applied in the field of ceramic matrix composite materials and forming, can solve problems such as limitations and complexity of forming process, and achieve the effects of high production efficiency, uniform density of structural components, and shortened degreasing time
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Embodiment 1
[0013] Commercial Al 2 o 3 Powder raw material, the average particle size of the particles is about 1μm, mixed with 5wt% ZrO 2 Nano powder, dissolve 20wt% of acrylamide and methylenebisacrylamide in deionized water to form a premix, the ratio of acrylamide and methylenebisacrylamide is 30:1, add 0.3 wt% Al 2 o 3 Organic dispersant of powder quality --- modified polyacrylic acid ammonium, then add 34vol% composite ceramic powder, and make a ceramic charge with viscosity <0.25Pas by stirring and ball milling, add 5ml ammonium persulfate to 1000g water Add the initiator to the billet, mix it evenly, and vacuum defoam, make SiC short fiber whiskers into a porous grid prefabricated body with a fiber content of 20%, put it in the mold, and then add the above-mentioned high solid content , Low-viscosity ceramic slurry is added to the feeding chamber of the injection machine. After the mold is closed, the fiber prefabricated body is injected, filled, and impregnated under pressure...
Embodiment 2
[0015] SiC powder, particle diameter is 0.6μm, and 3wt% (B 4 C+C) The powders are mixed, and 14wt% of ethylene oxide monomer and ethylene glycol are dissolved in deionized water to form a premixed liquid, and the ratio of ethylene oxide and ethylene glycol is 8:1. Add 0.3wt% dispersant of the mass of mixed ceramic powder --- tetramethylammonium hydroxide to the premixed liquid, and then add 57vol% volume fraction of composite ceramic powder, and make a dispersant with a viscosity of <0.25Pa·s by stirring ball milling The ceramic slurry is added in the blank according to the ratio of 1000g water plus Znil tetramethylethylenediamine.
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